4-[(4-acetyl-3-hydroxy-2-propylphenyl)methoxy]-β,β-dimethyl-δ-oxobenzenepentanoic acid

Base Information

Chemical Name:4-[(4-acetyl-3-hydroxy-2-propylphenyl)methoxy]-β,β-dimethyl-δ-oxobenzenepentanoic acid
CAS No.:119348-29-7
Molecular Formula:C₂₅H₃₀O₆
Molecular Weight:426.51
Hs Code.:

Synonyms:4-[(4-acetyl-3-hydroxy-2-propylphenyl)methoxy]-β,β-dimethyl-δ-oxobenzenepentanoic acid

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Chemical Property of 4-[(4-acetyl-3-hydroxy-2-propylphenyl)methoxy]-β,β-dimethyl-δ-oxobenzenepentanoic acid

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Technology Process of 4-[(4-acetyl-3-hydroxy-2-propylphenyl)methoxy]-β,β-dimethyl-δ-oxobenzenepentanoic acid

There total 7 articles about 4-[(4-acetyl-3-hydroxy-2-propylphenyl)methoxy]-β,β-dimethyl-δ-oxobenzenepentanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 119348-36-6
4-[(4-Acetyl-3-hydroxy-2-propylphenyl)methoxy]-β,β-dimethyl-δ-oxobenzenepentanoic acid, ethyl ester

: 119348-29-7
4-[(4-acetyl-3-hydroxy-2-propylphenyl)methoxy]-β,β-dimethyl-δ-oxobenzenepentanoic acid

Guidance literature:: With sodium hydroxide; In ethanol; for 2h; Heating;
DOI:10.1021/jm00113a014

Reference yield: 13.0%

: 119348-29-7
4-[(4-acetyl-3-hydroxy-2-propylphenyl)methoxy]-β,β-dimethyl-δ-oxobenzenepentanoic acid

Guidance literature:

Reference yield:

: 4160-82-1
3,3-dimethylglutaric anhydride

: 119348-29-7
4-[(4-acetyl-3-hydroxy-2-propylphenyl)methoxy]-β,β-dimethyl-δ-oxobenzenepentanoic acid

Guidance literature:: Multi-step reaction with 5 steps

1: aluminum chloride / CH₂Cl₂ / 3 h

2: 76 percent / pyridine hydrochloride / 20 h / 185 °C

3: 79 percent / methanesulfonic acid / 25 h / 25 °C

4: 78 percent / NaOEt, NaI / ethanol / 72 h

5: 85 percent / 5 N NaOH / ethanol / 2 h / Heating

With sodium hydroxide; aluminium trichloride; methanesulfonic acid; sodium ethanolate; pyridine hydrochloride; sodium iodide; In ethanol; dichloromethane;
DOI:10.1021/jm00113a014