ethyl 3,4-di-O-benzoyl-2-deoxy-1-thio-2-(2,2,2-trichloroethoxy)carbonylamino-β-D-glucopyranoside

Base Information

Chemical Name:ethyl 3,4-di-O-benzoyl-2-deoxy-1-thio-2-(2,2,2-trichloroethoxy)carbonylamino-β-D-glucopyranoside
CAS No.:1233488-71-5
Molecular Formula:C₂₅H₂₆Cl₃NO₈S
Molecular Weight:606.908
Hs Code.:

Synonyms:ethyl 3,4-di-O-benzoyl-2-deoxy-1-thio-2-(2,2,2-trichloroethoxy)carbonylamino-β-D-glucopyranoside

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Chemical Property of ethyl 3,4-di-O-benzoyl-2-deoxy-1-thio-2-(2,2,2-trichloroethoxy)carbonylamino-β-D-glucopyranoside

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Technology Process of ethyl 3,4-di-O-benzoyl-2-deoxy-1-thio-2-(2,2,2-trichloroethoxy)carbonylamino-β-D-glucopyranoside

There total 1 articles about ethyl 3,4-di-O-benzoyl-2-deoxy-1-thio-2-(2,2,2-trichloroethoxy)carbonylamino-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₄₄H₄₀Cl₃NO₈S

: 1233488-71-5
ethyl 3,4-di-O-benzoyl-2-deoxy-1-thio-2-(2,2,2-trichloroethoxy)carbonylamino-β-D-glucopyranoside

Guidance literature:: With trifluoroacetic acid; In dichloromethane;
DOI:10.1021/ol101089u

Reference yield: 99.0%

: 1233488-71-5
ethyl 3,4-di-O-benzoyl-2-deoxy-1-thio-2-(2,2,2-trichloroethoxy)carbonylamino-β-D-glucopyranoside

: 108-24-7
acetic anhydride

: ethyl 6-O-acetyl-3,4-di-O-benzoyl-2-deoxy-1-thio-2-(2,2,2-trichloroethoxycarbonylamino)-β-D-glucopyranoside

Guidance literature:: With pyridine; at 20 ℃; for 16h; Inert atmosphere;
DOI:10.1016/j.carres.2012.12.005

Reference yield: 90.0%

: 1233488-71-5
ethyl 3,4-di-O-benzoyl-2-deoxy-1-thio-2-(2,2,2-trichloroethoxy)carbonylamino-β-D-glucopyranoside

: 137334-39-5
6-O-acetyl-2,3,4-tri-O-benzoyl-α-D-glucopyranosyl bromide

: ethyl 6-O-acetyl-2,3,4-tri-O-benzoyl-β-D-glucopyranosyl-(1→6)-3,4-di-O-benzoyl-2-deoxy-1-thio-2-(2,2,2-trichloroethoxycarbonylamino)-β-D-glucopyranoside

Guidance literature:: With silver trifluoromethanesulfonate; In dichloromethane; at -20 - 20 ℃; for 1h; Molecular sieve; Inert atmosphere;
DOI:10.1016/j.carres.2012.12.005