Technology Process of 4-(14-(tetrahydropyran-2-yloxy)tetradecyloxy)phenylacetamidoxime
There total 3 articles about 4-(14-(tetrahydropyran-2-yloxy)tetradecyloxy)phenylacetamidoxime which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 97.3 percent / HCl / diethyl ether / 72 h / Heating
2: 61 percent / NaOH / ethanol; dimethylformamide / 20 °C
3: 57 percent / hydroxylamine hydrochloride; K2CO3 / ethanol / 18 h / Heating
With
hydrogenchloride; sodium hydroxide; hydroxylamine hydrochloride; potassium carbonate;
In
diethyl ether; ethanol; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2005.01.016
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 52.3 percent / HBr / heptane / 18 h / 90 °C
2: 97.3 percent / HCl / diethyl ether / 72 h / Heating
3: 61 percent / NaOH / ethanol; dimethylformamide / 20 °C
4: 57 percent / hydroxylamine hydrochloride; K2CO3 / ethanol / 18 h / Heating
With
hydrogenchloride; sodium hydroxide; hydroxylamine hydrochloride; hydrogen bromide; potassium carbonate;
In
diethyl ether; ethanol; n-heptane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2005.01.016
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 61 percent / NaOH / ethanol; dimethylformamide / 20 °C
2: 57 percent / hydroxylamine hydrochloride; K2CO3 / ethanol / 18 h / Heating
With
sodium hydroxide; hydroxylamine hydrochloride; potassium carbonate;
In
ethanol; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2005.01.016
