p-nitrophenyl 3-O-(4'-O-acetylferuloyl)-2,4-di-O-acetyl-β-D-xylopyranoside

Base Information

• Chemical Name: p-nitrophenyl 3-O-(4'-O-acetylferuloyl)-2,4-di-O-acetyl-β-D-xylopyranoside
• CAS No.: 1235988-93-8
• Molecular Formula: C₂₇H₂₇NO₁₃
• Molecular Weight: 573.51
• Mol file: 1235988-93-8.mol

Synonyms:p-nitrophenyl 3-O-(4'-O-acetylferuloyl)-2,4-di-O-acetyl-β-D-xylopyranoside

Chemical Property of p-nitrophenyl 3-O-(4'-O-acetylferuloyl)-2,4-di-O-acetyl-β-D-xylopyranoside

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of p-nitrophenyl 3-O-(4'-O-acetylferuloyl)-2,4-di-O-acetyl-β-D-xylopyranoside

There total 1 articles about p-nitrophenyl 3-O-(4'-O-acetylferuloyl)-2,4-di-O-acetyl-β-D-xylopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

4-acetoxy-3-methoxycinnamoyl chloride (50906-12-2) + 4-nitrophenyl 2,4-di-O-acetyl-β-D-xylopyranoside → p-nitrophenyl 3-O-(4'-O-acetylferuloyl)-2,4-di-O-acetyl-β-D-xylopyranoside (1235988-93-8)

Guidance literature:

With dmap; triethylamine; In dichloromethane; at 0 - 20 ℃;

DOI:10.1016/j.carres.2010.03.034

Reference yield: 63.0%

p-nitrophenyl 3-O-(4'-O-acetylferuloyl)-2,4-di-O-acetyl-β-D-xylopyranoside (1235988-93-8) → p-nitrophenyl 4-O-feruloyl-β-D-xylopyranoside (637761-31-0) + p-nitrophenyl 2-O-feruloyl-β-D-xylopyranoside (943833-75-8) + p-nitrophenyl 3-O-feruloyl-β-D-xylopyranoside (943833-77-0) + p-nitrophenyl β-D-xylopyranoside (2001-96-9)

Guidance literature:

With di(n-butyl)tin oxide; In methanol; dichloromethane; for 6h; chemoselective reaction; Reflux;

DOI:10.1016/j.carres.2010.03.034

upstream raw materials:

4-acetoxy-3-methoxycinnamoyl chloride

Downstream raw materials:

p-nitrophenyl 4-O-feruloyl-β-D-xylopyranoside

p-nitrophenyl 2-O-feruloyl-β-D-xylopyranoside

p-nitrophenyl 3-O-feruloyl-β-D-xylopyranoside

p-nitrophenyl β-D-xylopyranoside