dimethyl (2S,6R)-(+)-[2-(p-methoxybenzyl)-6-methylpiperidin-2-yl]phosphoate

Base Information

Chemical Name:dimethyl (2S,6R)-(+)-[2-(p-methoxybenzyl)-6-methylpiperidin-2-yl]phosphoate
CAS No.:406502-93-0
Molecular Formula:C₁₆H₂₆NO₄P
Molecular Weight:327.361
Hs Code.:

Synonyms:dimethyl (2S,6R)-(+)-[2-(p-methoxybenzyl)-6-methylpiperidin-2-yl]phosphoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of dimethyl (2S,6R)-(+)-[2-(p-methoxybenzyl)-6-methylpiperidin-2-yl]phosphoate

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Technology Process of dimethyl (2S,6R)-(+)-[2-(p-methoxybenzyl)-6-methylpiperidin-2-yl]phosphoate

There total 8 articles about dimethyl (2S,6R)-(+)-[2-(p-methoxybenzyl)-6-methylpiperidin-2-yl]phosphoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 406502-86-1
dimethyl (2R,6S,7R)-(-)-[7-(4-methoxy-phenyl)-2-methyl-1-aza-bicyclo-[4.1.0]hept-3-en-6-yl] phosphonate

: 406502-93-0
dimethyl (2S,6R)-(+)-[2-(p-methoxybenzyl)-6-methylpiperidin-2-yl]phosphoate

Guidance literature:: With hydrogen; palladium on activated charcoal; In tetrahydrofuran; for 6h;
DOI:10.1021/ol017289p

Reference yield: 80.0%

: 406502-92-9
dimethyl (2R,6S,7R)-(-)-[7-(4-methoxyphenyl)-2-methyl-1-aza-bicyclo[4.1.0]hept-6-yl] phosphonate

: 406502-93-0
dimethyl (2S,6R)-(+)-[2-(p-methoxybenzyl)-6-methylpiperidin-2-yl]phosphoate

Guidance literature:: With hydrogen; palladium on activated charcoal; In tetrahydrofuran; for 16h;
DOI:10.1021/ol017289p

Reference yield:

: 2004-70-8,17410-45-6,25212-15-1,64940-84-7
1-methylbuta-1,3-diene

: 406502-93-0
dimethyl (2S,6R)-(+)-[2-(p-methoxybenzyl)-6-methylpiperidin-2-yl]phosphoate

Guidance literature:: Multi-step reaction with 3 steps

1: 89 percent / toluene / 16 h / 20 °C

2: 40 percent / H₂ / Pd/C / methanol / 2 h

3: 80 percent / H₂ / Pd/C / tetrahydrofuran / 16 h

With hydrogen; palladium on activated charcoal; In tetrahydrofuran; methanol; toluene; 1: Diels-Alder reaction;
DOI:10.1021/ol017289p