5-[3-(3-Chloro-phenoxy)-propylamino]-2-isopropyl-2-(3,4,5-trimethoxy-phenyl)-pentanenitrile

Base Information

• Chemical Name: 5-[3-(3-Chloro-phenoxy)-propylamino]-2-isopropyl-2-(3,4,5-trimethoxy-phenyl)-pentanenitrile
• CAS No.: 103524-50-1
• Molecular Formula: C₂₆H₃₅ClN₂O₄
• Molecular Weight: 475.028

Synonyms:5-[3-(3-Chloro-phenoxy)-propylamino]-2-isopropyl-2-(3,4,5-trimethoxy-phenyl)-pentanenitrile

Chemical Property of 5-[3-(3-Chloro-phenoxy)-propylamino]-2-isopropyl-2-(3,4,5-trimethoxy-phenyl)-pentanenitrile

Chemical Property:

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Technology Process of 5-[3-(3-Chloro-phenoxy)-propylamino]-2-isopropyl-2-(3,4,5-trimethoxy-phenyl)-pentanenitrile

There total 1 articles about 5-[3-(3-Chloro-phenoxy)-propylamino]-2-isopropyl-2-(3,4,5-trimethoxy-phenyl)-pentanenitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

α-(2-formylethyl)-α-isopropyl-3,4,5-trimethoxybenzeneacetonitrile (66332-86-3) + 3-(3-chlorophenoxy)propylamine (116753-50-5) → 5-[3-(3-Chloro-phenoxy)-propylamino]-2-isopropyl-2-(3,4,5-trimethoxy-phenyl)-pentanenitrile (103524-50-1)

Guidance literature:

With sodium tetrahydroborate; Yield given. Multistep reaction; 1.) EtOH, 1.5 h, reflux, 2.) EtOH, ice water, 1 h, room temp.;

DOI:10.1248/cpb.36.373

Reference yield: 87.0%

formaldehyd (50-00-0,30525-89-4,61233-19-0) + 5-[3-(3-Chloro-phenoxy)-propylamino]-2-isopropyl-2-(3,4,5-trimethoxy-phenyl)-pentanenitrile (103524-50-1) → 5-{[3-(3-Chloro-phenoxy)-propyl]-methyl-amino}-2-isopropyl-2-(3,4,5-trimethoxy-phenyl)-pentanenitrile (103524-52-3)

Guidance literature:

With formic acid; In water; at 90 - 100 ℃; for 1h;

DOI:10.1248/cpb.36.373

Reference yield: 35.0%

formaldehyd (50-00-0,30525-89-4,61233-19-0) + 5-[3-(3-Chloro-phenoxy)-propylamino]-2-isopropyl-2-(3,4,5-trimethoxy-phenyl)-pentanenitrile (103524-50-1) → 2-Isopropyl-5-{methyl-[3-(3-nitro-phenoxy)-propyl]-amino}-2-(3,4,5-trimethoxy-phenyl)-pentanenitrile (103524-88-5)

Guidance literature:

With formic acid; In water; at 90 - 100 ℃; for 1h;

DOI:10.1248/cpb.36.373

upstream raw materials:

α-(2-formylethyl)-α-isopropyl-3,4,5-trimethoxybenzeneacetonitrile

3-(3-chlorophenoxy)propylamine

Downstream raw materials:

5-{[3-(3-Chloro-phenoxy)-propyl]-methyl-amino}-2-isopropyl-2-(3,4,5-trimethoxy-phenyl)-pentanenitrile

2-Isopropyl-5-{methyl-[3-(3-nitro-phenoxy)-propyl]-amino}-2-(3,4,5-trimethoxy-phenyl)-pentanenitrile

5-{[3-(3-Amino-phenoxy)-propyl]-methyl-amino}-2-isopropyl-2-(3,4,5-trimethoxy-phenyl)-pentanenitrile

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