C₃₁H₅₂O₇Si

Base Information

Chemical Name:C₃₁H₅₂O₇Si
CAS No.:934618-06-1
Molecular Formula:C₃₁H₅₂O₇Si
Molecular Weight:564.835
Hs Code.:

C<sub>31</sub>H<sub>52</sub>O<sub>7</sub>Si

Synonyms:C₃₁H₅₂O₇Si

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Chemical Property of C₃₁H₅₂O₇Si

Chemical Property:

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Technology Process of C₃₁H₅₂O₇Si

There total 22 articles about C₃₁H₅₂O₇Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 934618-05-0
C₃₇H₆₆O₇Si₂

: 934618-06-1
C₃₁H₅₂O₇Si

Guidance literature:: With water; acetic acid; In tetrahydrofuran;
DOI:10.1246/cl.2007.278

Reference yield:

: 934617-86-4
C₃₇H₆₈O₆SSi₂

: 934618-06-1
C₃₁H₅₂O₇Si

Guidance literature:: Multi-step reaction with 15 steps

1.1: 100 percent / TEA; DMAP / CH₂Cl₂

2.1: 94 percent / AcOH; H₂O / tetrahydrofuran / 50 °C

3.1: 98 percent / K₂CO₃ / methanol; CH₂Cl₂

4.1: 99 percent / MeI; NaHCO₃ / H₂O; acetone / 40 °C

5.1: 99 percent / H₂; quinoline / Lindlar cat. / ethyl acetate

6.1: 65 percent / Eu(fod)3 / xylene / 120 °C

7.1: 99 percent / AgNO₃; pyridine / acetonitrile

8.1: 94 percent / MCPBA; NaHCO₃ / CH₂Cl₂; H₂O / 0 °C

9.1: (PhSe)2; NaBH₄ / ethanol; butan-1-ol / Heating

9.2: 62 percent / H₂O₂; pyridine; 2-methyl-2-butene / CH₂Cl₂

10.1: 86 percent / MCPBA / CH₂Cl₂ / 0 °C

11.1: 97 percent / DMAP; TEA / CH₂Cl₂

12.1: (PhSe)2; NaBH₄ / ethanol; butan-1-ol / 50 °C

12.2: 38 percent / H₂O₂; pyridine; 2-methyl-2-butene / CH₂Cl₂

13.1: 59 percent / n-BuLi; DIBAL / toluene

14.1: 98 percent / TEA; DMAP / CH₂Cl₂

15.1: 93 percent / AcOH; H₂O / tetrahydrofuran

With pyridine; quinoline; dmap; sodium tetrahydroborate; n-butyllithium; TEA; diphenyl diselenide; water; hydrogen; diisobutylaluminium hydride; sodium hydrogencarbonate; potassium carbonate; silver nitrate; acetic acid; 3-chloro-benzenecarboperoxoic acid; Eu(fod)3; methyl iodide; Lindlar catalyst; In tetrahydrofuran; methanol; ethanol; dichloromethane; water; ethyl acetate; acetone; toluene; acetonitrile; xylene; butan-1-ol;
DOI:10.1246/cl.2007.278

Reference yield:

: 934618-00-5
C₃₁H₅₂O₅SSi

: 934618-06-1
C₃₁H₅₂O₇Si

Guidance literature:: Multi-step reaction with 12 steps

1.1: 99 percent / MeI; NaHCO₃ / H₂O; acetone / 40 °C

2.1: 99 percent / H₂; quinoline / Lindlar cat. / ethyl acetate

3.1: 65 percent / Eu(fod)3 / xylene / 120 °C

4.1: 99 percent / AgNO₃; pyridine / acetonitrile

5.1: 94 percent / MCPBA; NaHCO₃ / CH₂Cl₂; H₂O / 0 °C

6.1: (PhSe)2; NaBH₄ / ethanol; butan-1-ol / Heating

6.2: 62 percent / H₂O₂; pyridine; 2-methyl-2-butene / CH₂Cl₂

7.1: 86 percent / MCPBA / CH₂Cl₂ / 0 °C

8.1: 97 percent / DMAP; TEA / CH₂Cl₂

9.1: (PhSe)2; NaBH₄ / ethanol; butan-1-ol / 50 °C

9.2: 38 percent / H₂O₂; pyridine; 2-methyl-2-butene / CH₂Cl₂

10.1: 59 percent / n-BuLi; DIBAL / toluene

11.1: 98 percent / TEA; DMAP / CH₂Cl₂

12.1: 93 percent / AcOH; H₂O / tetrahydrofuran

With pyridine; quinoline; dmap; sodium tetrahydroborate; n-butyllithium; TEA; diphenyl diselenide; water; hydrogen; diisobutylaluminium hydride; sodium hydrogencarbonate; silver nitrate; acetic acid; 3-chloro-benzenecarboperoxoic acid; Eu(fod)3; methyl iodide; Lindlar catalyst; In tetrahydrofuran; ethanol; dichloromethane; water; ethyl acetate; acetone; toluene; acetonitrile; xylene; butan-1-ol;
DOI:10.1246/cl.2007.278