ε-((3S,4S)-4-((3S,4S)-4-((3S,4S)-4-amino-3-hydroxy-6-methylheptanoylamino)-5-cyclohexyl-3-hydroxypentanoylamino)-3-hydroxy-5-phenylpentanoylamino)hexanoic acid N-isoamylamide hydrochloride

Base Information

Chemical Name:ε-((3S,4S)-4-((3S,4S)-4-((3S,4S)-4-amino-3-hydroxy-6-methylheptanoylamino)-5-cyclohexyl-3-hydroxypentanoylamino)-3-hydroxy-5-phenylpentanoylamino)hexanoic acid N-isoamylamide hydrochloride
CAS No.:1309250-96-1
Molecular Formula:C₃₈H₇₃N₅O₇*ClH
Molecular Weight:748.488
Hs Code.:

ε-((3S,4S)-4-((3S,4S)-4-((3S,4S)-4-amino-3-hydroxy-6-methylheptanoylamino)-5-cyclohexyl-3-hydroxypentanoylamino)-3-hydroxy-5-phenylpentanoylamino)hexanoic acid N-isoamylamide hydrochloride

Synonyms:ε-((3S,4S)-4-((3S,4S)-4-((3S,4S)-4-amino-3-hydroxy-6-methylheptanoylamino)-5-cyclohexyl-3-hydroxypentanoylamino)-3-hydroxy-5-phenylpentanoylamino)hexanoic acid N-isoamylamide hydrochloride

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Chemical Property of ε-((3S,4S)-4-((3S,4S)-4-((3S,4S)-4-amino-3-hydroxy-6-methylheptanoylamino)-5-cyclohexyl-3-hydroxypentanoylamino)-3-hydroxy-5-phenylpentanoylamino)hexanoic acid N-isoamylamide hydrochloride

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Technology Process of ε-((3S,4S)-4-((3S,4S)-4-((3S,4S)-4-amino-3-hydroxy-6-methylheptanoylamino)-5-cyclohexyl-3-hydroxypentanoylamino)-3-hydroxy-5-phenylpentanoylamino)hexanoic acid N-isoamylamide hydrochloride

There total 12 articles about ε-((3S,4S)-4-((3S,4S)-4-((3S,4S)-4-amino-3-hydroxy-6-methylheptanoylamino)-5-cyclohexyl-3-hydroxypentanoylamino)-3-hydroxy-5-phenylpentanoylamino)hexanoic acid N-isoamylamide hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1309250-95-0
C₄₃H₈₁N₅O₉

: 1309250-96-1
ε-((3S,4S)-4-((3S,4S)-4-((3S,4S)-4-amino-3-hydroxy-6-methylheptanoylamino)-5-cyclohexyl-3-hydroxypentanoylamino)-3-hydroxy-5-phenylpentanoylamino)hexanoic acid N-isoamylamide hydrochloride

Guidance literature:: With hydrogenchloride; In 1,4-dioxane; at 20 ℃; for 0.5h;

Reference yield:

: 6404-29-1
6-(tert-butoxycarbonylamino)hexanoic acid

: 1309250-96-1
ε-((3S,4S)-4-((3S,4S)-4-((3S,4S)-4-amino-3-hydroxy-6-methylheptanoylamino)-5-cyclohexyl-3-hydroxypentanoylamino)-3-hydroxy-5-phenylpentanoylamino)hexanoic acid N-isoamylamide hydrochloride

Guidance literature:: Multi-step reaction with 6 steps

1: 4-methyl-morpholine; isobutyl chloroformate / tetrahydrofuran / 1.5 h / -15 - 20 °C / Inert atmosphere

2: hydrogenchloride / 1,4-dioxane / 0.5 h / 20 °C

3: benzotriazol-1-ol; dicyclohexyl-carbodiimide

4: hydrogenchloride / 1,4-dioxane / 0.5 h / 20 °C

5: benzotriazol-1-ol; dicyclohexyl-carbodiimide

6: hydrogenchloride / 1,4-dioxane / 0.5 h / 20 °C

With 4-methyl-morpholine; hydrogenchloride; benzotriazol-1-ol; dicyclohexyl-carbodiimide; isobutyl chloroformate; In tetrahydrofuran; 1,4-dioxane;

Reference yield:

: 58521-49-6
(3S,4S)-4-(tert-butoxycarbonylamino)-3-hydroxy-6-methylheptanoic acid

: 1309250-96-1
ε-((3S,4S)-4-((3S,4S)-4-((3S,4S)-4-amino-3-hydroxy-6-methylheptanoylamino)-5-cyclohexyl-3-hydroxypentanoylamino)-3-hydroxy-5-phenylpentanoylamino)hexanoic acid N-isoamylamide hydrochloride

Guidance literature:: Multi-step reaction with 4 steps

1: benzotriazol-1-ol; dicyclohexyl-carbodiimide

2: water / Alkaline conditions

3: benzotriazol-1-ol; dicyclohexyl-carbodiimide

4: hydrogenchloride / 1,4-dioxane / 0.5 h / 20 °C

With hydrogenchloride; water; benzotriazol-1-ol; dicyclohexyl-carbodiimide; In 1,4-dioxane;