N-(2-N-acetylamino-4-(3-aminophenyl)thiazole)-N-tert-butoxycarbonyltryptophanamide

Base Information

Chemical Name:N-(2-N-acetylamino-4-(3-aminophenyl)thiazole)-N-tert-butoxycarbonyltryptophanamide
CAS No.:1607464-90-3
Molecular Formula:C₂₇H₂₉N₅O₄S
Molecular Weight:519.624
Hs Code.:

Synonyms:N-(2-N-acetylamino-4-(3-aminophenyl)thiazole)-N-tert-butoxycarbonyltryptophanamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(2-N-acetylamino-4-(3-aminophenyl)thiazole)-N-tert-butoxycarbonyltryptophanamide

Chemical Property:

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Technology Process of N-(2-N-acetylamino-4-(3-aminophenyl)thiazole)-N-tert-butoxycarbonyltryptophanamide

There total 3 articles about N-(2-N-acetylamino-4-(3-aminophenyl)thiazole)-N-tert-butoxycarbonyltryptophanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 1607464-88-9
Nα-fluorenylmethyloxycarbonyl[N-(2-N-acetylamino-4-(3-aminophenyl)thiazole)]-N-tert-butoxycarbonyltryptophanamide

: 1607464-90-3
N-(2-N-acetylamino-4-(3-aminophenyl)thiazole)-N-tert-butoxycarbonyltryptophanamide

Guidance literature:: With pyridine; In dichloromethane; at 20 ℃; for 24h;
DOI:10.1002/chem.201303664

Reference yield:

: 143824-78-6,163619-04-3
3-[(S)-2-carboxy-2-(9H-fluoren-9-ylmethoxycarbonylamino)ethyl]indole-1-carboxylic acid tert-butyl ester

: 1607464-90-3
N-(2-N-acetylamino-4-(3-aminophenyl)thiazole)-N-tert-butoxycarbonyltryptophanamide

Guidance literature:: Multi-step reaction with 2 steps

1: 2-chloro-1-methyl-pyridinium iodide; triethylamine / dichloromethane / 3 h / Reflux

2: pyridine / dichloromethane / 24 h / 20 °C

With pyridine; 2-chloro-1-methyl-pyridinium iodide; triethylamine; In dichloromethane;
DOI:10.1002/chem.201303664

Reference yield:

: 134812-30-9
N-(4-(3'-aminophenyl)thiazol-2-yl)acetamide

: 1607464-90-3
N-(2-N-acetylamino-4-(3-aminophenyl)thiazole)-N-tert-butoxycarbonyltryptophanamide

Guidance literature:: Multi-step reaction with 2 steps

1: 2-chloro-1-methyl-pyridinium iodide; triethylamine / dichloromethane / 3 h / Reflux

2: pyridine / dichloromethane / 24 h / 20 °C

With pyridine; 2-chloro-1-methyl-pyridinium iodide; triethylamine; In dichloromethane;
DOI:10.1002/chem.201303664