methyl 2,5-di-O-benzoyl-α-D-arabinofuranosyl-(1->5)-2,3-di-O-benzoyl-α-D-arabinofuranoside

Base Information

Chemical Name:methyl 2,5-di-O-benzoyl-α-D-arabinofuranosyl-(1->5)-2,3-di-O-benzoyl-α-D-arabinofuranoside
CAS No.:1359987-88-4
Molecular Formula:C₃₉H₃₆O₁₃
Molecular Weight:712.707
Hs Code.:

Synonyms:methyl 2,5-di-O-benzoyl-α-D-arabinofuranosyl-(1->5)-2,3-di-O-benzoyl-α-D-arabinofuranoside

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Chemical Property of methyl 2,5-di-O-benzoyl-α-D-arabinofuranosyl-(1->5)-2,3-di-O-benzoyl-α-D-arabinofuranoside

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Technology Process of methyl 2,5-di-O-benzoyl-α-D-arabinofuranosyl-(1->5)-2,3-di-O-benzoyl-α-D-arabinofuranoside

There total 4 articles about methyl 2,5-di-O-benzoyl-α-D-arabinofuranosyl-(1->5)-2,3-di-O-benzoyl-α-D-arabinofuranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 1359987-82-8
phenyl 2,5-di-O-benzoyl-1-thio-α-D-arabinofuranoside

: 204918-51-4
methyl 2,3-di-O-benzoyl-α-D-arabinofuranoside

: 1359987-88-4
methyl 2,5-di-O-benzoyl-α-D-arabinofuranosyl-(1->5)-2,3-di-O-benzoyl-α-D-arabinofuranoside

Guidance literature:: With N-iodo-succinimide; trifluorormethanesulfonic acid; In dichloromethane; at -40 - -20 ℃; for 0.5h; Inert atmosphere; Molecular sieve;
DOI:10.1021/jo300084g

Reference yield:

: 1359987-80-6
methyl 2,5-di-O-benzoyl-3-O-tert-butyldiphenylsilyl-α-D-arabinofuranoside

: 1359987-88-4
methyl 2,5-di-O-benzoyl-α-D-arabinofuranosyl-(1->5)-2,3-di-O-benzoyl-α-D-arabinofuranoside

Guidance literature:: Multi-step reaction with 3 steps

1: boron trifluoride diethyl etherate / dichloromethane / 8 h / 0 - 20 °C / Inert atmosphere

2: tetrabutyl ammonium fluoride / tetrahydrofuran / 3 h / 0 - 15 °C / Inert atmosphere

3: N-iodo-succinimide; trifluorormethanesulfonic acid / dichloromethane / 0.5 h / -40 - -20 °C / Inert atmosphere; Molecular sieve

With N-iodo-succinimide; trifluorormethanesulfonic acid; boron trifluoride diethyl etherate; tetrabutyl ammonium fluoride; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jo300084g

Reference yield:

: 1359987-81-7
phenyl 2,5-di-O-benzoyl-3-O-tert-butyldiphenylsilyl-1-thio-α-D-arabinofuranoside

: 1359987-88-4
methyl 2,5-di-O-benzoyl-α-D-arabinofuranosyl-(1->5)-2,3-di-O-benzoyl-α-D-arabinofuranoside

Guidance literature:: Multi-step reaction with 2 steps

1: tetrabutyl ammonium fluoride / tetrahydrofuran / 3 h / 0 - 15 °C / Inert atmosphere

2: N-iodo-succinimide; trifluorormethanesulfonic acid / dichloromethane / 0.5 h / -40 - -20 °C / Inert atmosphere; Molecular sieve

With N-iodo-succinimide; trifluorormethanesulfonic acid; tetrabutyl ammonium fluoride; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jo300084g