Technology Process of C21H22N6O2
There total 4 articles about C21H22N6O2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C26H28N6O3;
With
hydrido(dimethylphosphinous acid κP)[hydrogen bis(dimethylphosphinito-κP)]platinum(II);
In
ethanol; water;
at 80 ℃;
With
trifluoroacetic acid;
In
dichloromethane;
at 20 ℃;
for 3h;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: triethylamine; dmap / dichloromethane / 24 h
2.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 18 h / 70 °C
3.1: hydrido(dimethylphosphinous acid κP)[hydrogen bis(dimethylphosphinito-κP)]platinum(II) / water; ethanol / 80 °C
3.2: 3 h / 20 °C
With
dmap; hydrido(dimethylphosphinous acid κP)[hydrogen bis(dimethylphosphinito-κP)]platinum(II); sodium hydride; triethylamine;
In
ethanol; dichloromethane; water; N,N-dimethyl-formamide; mineral oil;
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 18 h / 70 °C
2.1: hydrido(dimethylphosphinous acid κP)[hydrogen bis(dimethylphosphinito-κP)]platinum(II) / water; ethanol / 80 °C
2.2: 3 h / 20 °C
With
hydrido(dimethylphosphinous acid κP)[hydrogen bis(dimethylphosphinito-κP)]platinum(II); sodium hydride;
In
ethanol; water; N,N-dimethyl-formamide; mineral oil;