phenylmethyl <2,3,9,9a-tetrahydro-2-(2-methylpropyl)-3-oxo-1-<(phenylmethoxy)carbonyl>-9-<(5,6,7,13-tetrahydro-5,13-dioxoquinazolino<3,2-a><1,4>benzodiazepin-7-yl)methyl>1H-imidazo<1,2-a>indol-9-yl>butanedioic acid ester

Base Information

Chemical Name:phenylmethyl <2,3,9,9a-tetrahydro-2-(2-methylpropyl)-3-oxo-1-<(phenylmethoxy)carbonyl>-9-<(5,6,7,13-tetrahydro-5,13-dioxoquinazolino<3,2-a><1,4>benzodiazepin-7-yl)methyl>1H-imidazo<1,2-a>indol-9-yl>butanedioic acid ester
CAS No.:103241-33-4
Molecular Formula:C₅₀H₄₅N₅O₉
Molecular Weight:859.935
Hs Code.:

phenylmethyl <2,3,9,9a-tetrahydro-2-(2-methylpropyl)-3-oxo-1-<(phenylmethoxy)carbonyl>-9-<(5,6,7,13-tetrahydro-5,13-dioxoquinazolino<3,2-a><1,4>benzodiazepin-7-yl)methyl>1H-imidazo<1,2-a>indol-9-yl>butanedioic acid ester

Synonyms:phenylmethyl <2,3,9,9a-tetrahydro-2-(2-methylpropyl)-3-oxo-1-<(phenylmethoxy)carbonyl>-9-<(5,6,7,13-tetrahydro-5,13-dioxoquinazolino<3,2-a><1,4>benzodiazepin-7-yl)methyl>1H-imidazo<1,2-a>indol-9-yl>butanedioic acid ester

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Chemical Property of phenylmethyl <2,3,9,9a-tetrahydro-2-(2-methylpropyl)-3-oxo-1-<(phenylmethoxy)carbonyl>-9-<(5,6,7,13-tetrahydro-5,13-dioxoquinazolino<3,2-a><1,4>benzodiazepin-7-yl)methyl>1H-imidazo<1,2-a>indol-9-yl>butanedioic acid ester

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Technology Process of phenylmethyl <2,3,9,9a-tetrahydro-2-(2-methylpropyl)-3-oxo-1-<(phenylmethoxy)carbonyl>-9-<(5,6,7,13-tetrahydro-5,13-dioxoquinazolino<3,2-a><1,4>benzodiazepin-7-yl)methyl>1H-imidazo<1,2-a>indol-9-yl>butanedioic acid ester

There total 3 articles about phenylmethyl <2,3,9,9a-tetrahydro-2-(2-methylpropyl)-3-oxo-1-<(phenylmethoxy)carbonyl>-9-<(5,6,7,13-tetrahydro-5,13-dioxoquinazolino<3,2-a><1,4>benzodiazepin-7-yl)methyl>1H-imidazo<1,2-a>indol-9-yl>butanedioic acid ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 36.0%

: 103-40-2
succinic acid monobenzyl ester

: 102743-51-1
phenylmethyl 2,3,9,9a-tetrahydro-9-hydroxy-2-(2-methylpropyl)-3-oxo-9-[(5,6,7,13-tetrahydro-5,13-dioxoquinazolino[3,2-a][1,4]benzodiazepin-7-yl)methyl]-1H-imidazo[1,2-a]indole-1-carboxylic acid ester

: 103241-33-4
phenylmethyl <2,3,9,9a-tetrahydro-2-(2-methylpropyl)-3-oxo-1-<(phenylmethoxy)carbonyl>-9-<(5,6,7,13-tetrahydro-5,13-dioxoquinazolino<3,2-a><1,4>benzodiazepin-7-yl)methyl>1H-imidazo<1,2-a>indol-9-yl>butanedioic acid ester

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; Ambient temperature;
DOI:10.1021/jm00160a024

Reference yield:

: 501-53-1,94274-21-2
benzyl chloroformate

: 103241-33-4
phenylmethyl <2,3,9,9a-tetrahydro-2-(2-methylpropyl)-3-oxo-1-<(phenylmethoxy)carbonyl>-9-<(5,6,7,13-tetrahydro-5,13-dioxoquinazolino<3,2-a><1,4>benzodiazepin-7-yl)methyl>1H-imidazo<1,2-a>indol-9-yl>butanedioic acid ester

Guidance literature:: Multi-step reaction with 2 steps

1: 88 percent / 4-(dimethylamino)pyridine / CH₂Cl₂ / 20 h / Ambient temperature

2: 36 percent / 4-(dimethylamino)pyridine, dicyclohexylcarbodiimide / CH₂Cl₂ / Ambient temperature

With dmap; dicyclohexyl-carbodiimide; In dichloromethane;
DOI:10.1021/jm00160a024

Reference yield:

: 93413-04-8
Asperlicin

: 103241-33-4
phenylmethyl <2,3,9,9a-tetrahydro-2-(2-methylpropyl)-3-oxo-1-<(phenylmethoxy)carbonyl>-9-<(5,6,7,13-tetrahydro-5,13-dioxoquinazolino<3,2-a><1,4>benzodiazepin-7-yl)methyl>1H-imidazo<1,2-a>indol-9-yl>butanedioic acid ester

Guidance literature:: Multi-step reaction with 2 steps

1: 88 percent / 4-(dimethylamino)pyridine / CH₂Cl₂ / 20 h / Ambient temperature

2: 36 percent / 4-(dimethylamino)pyridine, dicyclohexylcarbodiimide / CH₂Cl₂ / Ambient temperature

With dmap; dicyclohexyl-carbodiimide; In dichloromethane;
DOI:10.1021/jm00160a024