ruthenoceno[a]acenaphthylene

Base Information

Chemical Name:ruthenoceno[a]acenaphthylene
CAS No.:473926-59-9
Molecular Formula:C₂₀H₁₄Ru
Molecular Weight:355.401
Hs Code.:

Synonyms:ruthenoceno[a]acenaphthylene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of ruthenoceno[a]acenaphthylene

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Technology Process of ruthenoceno[a]acenaphthylene

There total 1 articles about ruthenoceno[a]acenaphthylene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 3.0%

: 473926-52-2
2-ruthenocenyl-4,4,5,5-tetramethyl-1,3-dioxa-2-borolane

: 1730-04-7
1,8-diiodonaphthalene

: 1287-13-4
bis(η⁵-cyclopentadienyl)ruthenium

: 112461-16-2
1,8-bis(ruthenocenyl)naphthalene

: 473926-59-9
ruthenoceno[a]acenaphthylene

Guidance literature:: With Cs₂(CO)3; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In N,N-dimethyl-formamide; under Ar; soln. of Ru complex and 1,8-diiodonaphthalene (molar ratio 2.3:1) in DMF bubbled with N2 (20 min); Pd(PPh3)4 and Cs2(CO)3 (2.3 equiv.)added; heated at 90°C for 4 h; accordingly to T. Watanabe, N. Mi yaura, A. Suzuki, Synlett (1992) 207; diluted with benzene; washed with water and concd. aq. LiCl; dried over MgSO4; evapd. by evaporator; cromd. (SiO2, hexane-benzene); elem. anal.;
DOI:10.1016/S0022-328X(02)01407-9