1-methyl, 6-benzyl (S)-2-tert-butoxycarbonylamino-5-benzyloxycarbonylhexanedicarboxylate

Base Information

Chemical Name:1-methyl, 6-benzyl (S)-2-tert-butoxycarbonylamino-5-benzyloxycarbonylhexanedicarboxylate
CAS No.:868285-82-9
Molecular Formula:C₂₇H₃₃NO₈
Molecular Weight:499.561
Hs Code.:

Synonyms:1-methyl, 6-benzyl (S)-2-tert-butoxycarbonylamino-5-benzyloxycarbonylhexanedicarboxylate

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Chemical Property of 1-methyl, 6-benzyl (S)-2-tert-butoxycarbonylamino-5-benzyloxycarbonylhexanedicarboxylate

Chemical Property:

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Technology Process of 1-methyl, 6-benzyl (S)-2-tert-butoxycarbonylamino-5-benzyloxycarbonylhexanedicarboxylate

There total 1 articles about 1-methyl, 6-benzyl (S)-2-tert-butoxycarbonylamino-5-benzyloxycarbonylhexanedicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 15014-25-2
malonic acid dibenzyl ester

: 101650-14-0
methyl (2S)-2-(tert-butoxycarbonyl)amino-4-iodobutanoate

: 868285-82-9
1-methyl, 6-benzyl (S)-2-tert-butoxycarbonylamino-5-benzyloxycarbonylhexanedicarboxylate

Guidance literature:: malonic acid dibenzyl ester; With sodium hydride; In N,N-dimethyl-formamide; at 20 ℃;

methyl (2S)-2-(tert-butoxycarbonyl)amino-4-iodobutanoate; In N,N-dimethyl-formamide; at 70 ℃; for 20h;

Reference yield:

: 4548-45-2
2-chloro-5-nitropyridine

: 868285-82-9
1-methyl, 6-benzyl (S)-2-tert-butoxycarbonylamino-5-benzyloxycarbonylhexanedicarboxylate

: 868285-85-2
6-benzyl, 1-methyl (S)-2-tert-butoxycarbonylamino-5-benzyloxycarbonyl-5-(5-nitropyridin-2-yl)hexane dicarboxylate

Guidance literature:: 1-methyl, 6-benzyl (S)-2-tert-butoxycarbonylamino-5-benzyloxycarbonylhexanedicarboxylate; With sodium hydride; In tetrahydrofuran; at 20 ℃;

2-chloro-5-nitropyridine; In tetrahydrofuran; at 60 ℃; for 24h; Product distribution / selectivity;