1-<(4-Methoxyphenyl)sulfonyl>-1,2,2a,3-tetrahydrobenzindole

Base Information

Chemical Name:1-<(4-Methoxyphenyl)sulfonyl>-1,2,2a,3-tetrahydrobenzindole
CAS No.:134745-86-1
Molecular Formula:C₁₈H₁₇NO₃S
Molecular Weight:327.404
Hs Code.:

1-<(4-Methoxyphenyl)sulfonyl>-1,2,2a,3-tetrahydrobenz<cd>indole

Synonyms:1-<(4-Methoxyphenyl)sulfonyl>-1,2,2a,3-tetrahydrobenzindole

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-<(4-Methoxyphenyl)sulfonyl>-1,2,2a,3-tetrahydrobenzindole

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of 1-<(4-Methoxyphenyl)sulfonyl>-1,2,2a,3-tetrahydrobenzindole

There total 1 articles about 1-<(4-Methoxyphenyl)sulfonyl>-1,2,2a,3-tetrahydrobenzindole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 124465-55-0,51867-05-1
1-benzoyl-1,2,2a,3-tetrahydro-benz[cd]indole

: 134745-86-1
1-<(4-Methoxyphenyl)sulfonyl>-1,2,2a,3-tetrahydrobenzindole

Guidance literature:: Multi-step reaction with 2 steps

1: conc. hydrochloric acid / 8 h / Heating

2: triethylamine / benzene / 5 h / Heating

With hydrogenchloride; triethylamine; In benzene;
DOI:10.1248/cpb.39.23

Reference yield: 90.0%

: 134745-86-1
1-<(4-Methoxyphenyl)sulfonyl>-1,2,2a,3-tetrahydrobenzindole

: 134745-87-2
4,5-Epoxy-1,2,2a,3,4,5-hexahydro-1-<(4-methoxyphenyl)sulfonyl>benzindole

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In chloroform; at 5 ℃; for 3h;
DOI:10.1248/cpb.39.23

Reference yield:

: 134745-86-1
1-<(4-Methoxyphenyl)sulfonyl>-1,2,2a,3-tetrahydrobenzindole

: 548-42-5,82597-81-7,89708-38-3,95586-10-0,194346-16-2
(+/-)-Agroclavine

Guidance literature:: Multi-step reaction with 11 steps

1: 90 percent / m-chloroperbenzoic acid / CHCl₃ / 3 h / 5 °C

2: 93 percent / p-toluenesulfonic acid / toluene / 1 h / Heating

3: toluene / 6 h / Heating

4: triethylamine / toluene; benzene / 2 h / Heating

5: 53 percent / sodium borohydride / benzene; methanol / 2 h / 5 °C / Irradiation

6: 1.) ozone, 2.) lithium aluminum hydride / 1.) methylene dichloride, -30 deg C, 10 min, 2.) THF, ether, reflux, 2 h

7: 89 percent / pyridine / 3.5 h / 0 °C

8: 74 percent / sodium borohydride / dimethylsulfoxide / 8 h / 80 °C

9: 24 percent / thionyl chloride / benzene / 1.5 h / Heating

10: 94 percent / sodium, liquid ammonia / tetrahydrofuran / 1 h

11: 89 percent / phenylseleninic anhydride, indole / tetrahydrofuran / 1.5 h / 40 °C

With pyridine; indole; sodium tetrahydroborate; lithium aluminium tetrahydride; thionyl chloride; benzeneseleninic anhydride; ammonia; sodium; toluene-4-sulfonic acid; ozone; triethylamine; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; methanol; chloroform; dimethyl sulfoxide; toluene; benzene;
DOI:10.1248/cpb.39.23