Technology Process of C26H21BrO2
There total 1 articles about C26H21BrO2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
2-bromoanthracene-9,10-dione; phenyllithium;
In
diethyl ether; dibutyl ether; toluene;
at -20 ℃;
for 6h;
With
water;
In
diethyl ether; dibutyl ether; toluene;
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: potassium iodide; acetic acid; sodium hypophosphite monohydrate / 6 h / Reflux
2.1: n-butyllithium / hexane; tetrahydrofuran / -80 °C
2.2: 2 h
2.3: 12 h
With
n-butyllithium; sodium hypophosphite monohydrate; acetic acid; potassium iodide;
In
tetrahydrofuran; hexane;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: potassium iodide; acetic acid; sodium hypophosphite monohydrate / 6 h / Reflux
2.1: n-butyllithium / hexane; tetrahydrofuran / -80 °C
2.2: 2 h
2.3: 12 h
3.1: sodium carbonate / tetrakis(triphenylphosphine) palladium(0) / toluene; ethanol; water / 12 h / 90 °C
With
n-butyllithium; sodium hypophosphite monohydrate; sodium carbonate; acetic acid; potassium iodide;
tetrakis(triphenylphosphine) palladium(0);
In
tetrahydrofuran; ethanol; hexane; water; toluene;