tert-butyl 4-(3-(2-chlorophenyl)-5-methylisoxazole-4-carbonyl)piperazine-1-carboxylate

Base Information

Chemical Name:tert-butyl 4-(3-(2-chlorophenyl)-5-methylisoxazole-4-carbonyl)piperazine-1-carboxylate
CAS No.:1370419-31-0
Molecular Formula:C₂₀H₂₄ClN₃O₄
Molecular Weight:405.881
Hs Code.:

Synonyms:tert-butyl 4-(3-(2-chlorophenyl)-5-methylisoxazole-4-carbonyl)piperazine-1-carboxylate

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Chemical Property of tert-butyl 4-(3-(2-chlorophenyl)-5-methylisoxazole-4-carbonyl)piperazine-1-carboxylate

Chemical Property:

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Technology Process of tert-butyl 4-(3-(2-chlorophenyl)-5-methylisoxazole-4-carbonyl)piperazine-1-carboxylate

There total 2 articles about tert-butyl 4-(3-(2-chlorophenyl)-5-methylisoxazole-4-carbonyl)piperazine-1-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 25629-50-9
3-(2-chlorophenyl)-5-methylisoxazole-4-carbonyl chloride

: 57260-71-6
1-t-Butoxycarbonylpiperazine

: 1370419-31-0
tert-butyl 4-(3-(2-chlorophenyl)-5-methylisoxazole-4-carbonyl)piperazine-1-carboxylate

Guidance literature:: With triethylamine; In dichloromethane;

Reference yield:

: 23598-72-3
3-(2-chlorophenyl)-5-methyl-4-isoxazolecarboxylic acid

: 1370419-31-0
tert-butyl 4-(3-(2-chlorophenyl)-5-methylisoxazole-4-carbonyl)piperazine-1-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: N,N-dimethyl-formamide; oxalyl dichloride / dichloromethane / 2 h

2: triethylamine / dichloromethane

With oxalyl dichloride; triethylamine; N,N-dimethyl-formamide; In dichloromethane;

Reference yield:

: 1370419-31-0
tert-butyl 4-(3-(2-chlorophenyl)-5-methylisoxazole-4-carbonyl)piperazine-1-carboxylate

: 1370419-39-8
(3-(2-chlorophenyl)-5-methylisoxazol-4-yl)(4-(3-methoxy-5-nitropyridin-2-yl)piperazin-1-yl)methanone

Guidance literature:: Multi-step reaction with 2 steps

1: trifluoroacetic acid / dichloromethane / 2 h

2: tetrahydrofuran / 20 °C

With trifluoroacetic acid; In tetrahydrofuran; dichloromethane;