[(Ph3Sb)2(μ-O)(μ-1,1,2,3,3-pentamethyltrimethylene phosphinate)2]

Base Information

Chemical Name:[(Ph3Sb)2(μ-O)(μ-1,1,2,3,3-pentamethyltrimethylene phosphinate)2]
CAS No.:1147306-40-8
Molecular Formula:C₅₂H₆₂O₅P₂Sb₂
Molecular Weight:1072.51
Hs Code.:

Synonyms:[(Ph3Sb)2(μ-O)(μ-1,1,2,3,3-pentamethyltrimethylene phosphinate)2]

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Chemical Property of [(Ph3Sb)2(μ-O)(μ-1,1,2,3,3-pentamethyltrimethylene phosphinate)2]

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Technology Process of [(Ph3Sb)2(μ-O)(μ-1,1,2,3,3-pentamethyltrimethylene phosphinate)2]

There total 1 articles about [(Ph3Sb)2(μ-O)(μ-1,1,2,3,3-pentamethyltrimethylene phosphinate)2] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: triphenylantimony dichloride monohydrate

: 17405-93-5,17405-94-6,35210-25-4
1,1,2,3,3-pentamethyltrimethylene phosphinic acid

: 1147306-40-8
[(Ph3Sb)2(μ-O)(μ-1,1,2,3,3-pentamethyltrimethylene phosphinate)2]

Guidance literature:: With Et₃N; In benzene; Sb compd. was added to soln. of P acid and Et3N (2 equiv.) in C6H6; stirred for 24 h; filtered; evapd.; recrystd. (hexane); elem. anal.;
DOI:10.1021/om900113q

Reference yield: 32.0%

: 1147306-40-8
[(Ph3Sb)2(μ-O)(μ-1,1,2,3,3-pentamethyltrimethylene phosphinate)2]

: 7732-18-5
water

: 75-05-8,26809-02-9
acetonitrile

: [(Ph2Sb)2(PhSb)7(μ-O)11(μ3-O)3(μ-OH)(μ-1,1,2,3,3-pentamethyltrimethylene phosphinate)2]

Guidance literature:: In water; acetonitrile; Sb compd. was dissolved in MeCN/H2O (99/1) at 50°C; filtered; slowly evapd. at 45°C for few wk; elem. anal.;
DOI:10.1021/om900113q