C₁₈H₂₄O₅

Base Information

• Chemical Name: C₁₈H₂₄O₅
• CAS No.: 1427031-97-7
• Molecular Formula: C₁₈H₂₄O₅
• Molecular Weight: 320.386
• Mol file: 1427031-97-7.mol

Synonyms:C₁₈H₂₄O₅

Chemical Property of C₁₈H₂₄O₅

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₈H₂₄O₅

There total 1 articles about C₁₈H₂₄O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

C23H36O5Si → C18H24O5 (1427031-97-7)

Guidance literature:

With pyridinium p-toluenesulfonate; In methanol; at 20 ℃; for 22h;

DOI:10.1021/ol400408w

Reference yield: 85.0%

C18H24O5 (1427031-97-7) + O-(4-methoxybenzyl)-trichloroacetimidate (89238-99-3) → C26H32O6 (1427031-98-8)

Guidance literature:

With lanthanum(lll) triflate; In toluene; at 20 ℃; for 1h;

DOI:10.1021/ol400408w

Reference yield:

C18H24O5 (1427031-97-7) → C51H76O8Si2 (1427032-04-9)

Guidance literature:

Multi-step reaction with 7 steps

1: lanthanum(lll) triflate / toluene / 1 h / 20 °C

2: 4-methylmorpholine N-oxide; osmium(VIII) oxide / tetrahydrofuran; water; tert-butyl alcohol / 20 °C

3: sodium periodate / tetrahydrofuran; water / 1 h / 0 - 20 °C

4: chromium dichloride / tetrahydrofuran; N,N-dimethyl-formamide / 4 h / 20 °C

5: lithium hydroxide monohydrate / tetrahydrofuran; water; methanol / 0 - 20 °C

6: triethylamine / tetrahydrofuran / 0.83 h / 0 - 20 °C

7: dmap / toluene / 1.5 h / 20 °C

With chromium dichloride; dmap; sodium periodate; osmium(VIII) oxide; lithium hydroxide monohydrate; 4-methylmorpholine N-oxide; triethylamine; lanthanum(lll) triflate; In tetrahydrofuran; methanol; water; N,N-dimethyl-formamide; toluene; tert-butyl alcohol; 4: |Takai-Utimoto Olefination / 6: |Yamaguchi Lactonization;

DOI:10.1021/ol400408w

Downstream raw materials:

C₂₅H₃₀O₆

C₁₉H₂₆O₇

C₂₀H₂₈O₆

C₁₉H₂₆O₆