C₂₁H₂₂ClN₃O₅

Base Information

Chemical Name:C₂₁H₂₂ClN₃O₅
CAS No.:1622396-69-3
Molecular Formula:C₂₁H₂₂ClN₃O₅
Molecular Weight:431.876
Hs Code.:

C<sub>21</sub>H<sub>22</sub>ClN<sub>3</sub>O<sub>5</sub>

Synonyms:C₂₁H₂₂ClN₃O₅

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Chemical Property of C₂₁H₂₂ClN₃O₅

Chemical Property:

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Technology Process of C₂₁H₂₂ClN₃O₅

There total 11 articles about C₂₁H₂₂ClN₃O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.9%

: 1622317-18-3
ethyl 4-(4-chloro-6-methoxyquinazolin-7-yloxy)butanoate

: 52671-64-4
4-Amino-3-chlorophenol hydrochloride

: 1622396-69-3
C₂₁H₂₂ClN₃O₅

Guidance literature:: With caesium carbonate; In acetonitrile; at 50 ℃; for 2h;

Reference yield:

: 3943-74-6
4-hydroxy-3-methoxybenzoic acid methyl ester

: 1622396-69-3
C₂₁H₂₂ClN₃O₅

Guidance literature:: Multi-step reaction with 10 steps

1: potassium carbonate / N,N-dimethyl-formamide / 3 h / 100 °C

2: nitric acid; acetic acid / 0.33 h / -10 °C

3: iron; ammonium chloride / water; methanol / 105 °C

4: ammonium acetate; methanol / 100 °C

5: methanesulfonic acid; trifluoroacetic acid / 3 h / Reflux

6: pyridine / 3 h / 120 °C

7: thionyl chloride / N,N-dimethyl-formamide / 1.5 h / Reflux

8: methanol; ammonia / dichloromethane / 0.17 h / 80 °C

9: potassium carbonate / tetrahydrofuran / 20 °C

10: caesium carbonate / acetonitrile / 2 h / 50 °C

With pyridine; methanol; thionyl chloride; methanesulfonic acid; ammonium acetate; ammonia; nitric acid; iron; potassium carbonate; ammonium chloride; caesium carbonate; acetic acid; trifluoroacetic acid; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile;

Reference yield:

: 61032-41-5
methyl 4-(benzyloxy)-5-methoxy-2-nitrobenzoate

: 1622396-69-3
C₂₁H₂₂ClN₃O₅

Guidance literature:: Multi-step reaction with 8 steps

1: iron; ammonium chloride / water; methanol / 105 °C

2: ammonium acetate; methanol / 100 °C

3: methanesulfonic acid; trifluoroacetic acid / 3 h / Reflux

4: pyridine / 3 h / 120 °C

5: thionyl chloride / N,N-dimethyl-formamide / 1.5 h / Reflux

6: methanol; ammonia / dichloromethane / 0.17 h / 80 °C

7: potassium carbonate / tetrahydrofuran / 20 °C

8: caesium carbonate / acetonitrile / 2 h / 50 °C

With pyridine; methanol; thionyl chloride; methanesulfonic acid; ammonium acetate; ammonia; iron; potassium carbonate; ammonium chloride; caesium carbonate; trifluoroacetic acid; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile;