12-chloro-7-(p-chlorophenyl)-10-oxo-indeno<1,2-b>-1,2,5-oxadiazolo<3,4-d>pyridine

Base Information

Chemical Name:12-chloro-7-(p-chlorophenyl)-10-oxo-indeno<1,2-b>-1,2,5-oxadiazolo<3,4-d>pyridine
CAS No.:225795-65-3
Molecular Formula:C₁₈H₇Cl₂N₃O₂
Molecular Weight:368.178
Hs Code.:

Synonyms:12-chloro-7-(p-chlorophenyl)-10-oxo-indeno<1,2-b>-1,2,5-oxadiazolo<3,4-d>pyridine

Suppliers and Price of 12-chloro-7-(p-chlorophenyl)-10-oxo-indeno<1,2-b>-1,2,5-oxadiazolo<3,4-d>pyridine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 12-chloro-7-(p-chlorophenyl)-10-oxo-indeno<1,2-b>-1,2,5-oxadiazolo<3,4-d>pyridine

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 12-chloro-7-(p-chlorophenyl)-10-oxo-indeno<1,2-b>-1,2,5-oxadiazolo<3,4-d>pyridine

There total 4 articles about 12-chloro-7-(p-chlorophenyl)-10-oxo-indeno<1,2-b>-1,2,5-oxadiazolo<3,4-d>pyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 2.0%

: 225795-70-0
4,7-di(p-chlorophenyl)-6-ethoxycarbonyl-1,2,5-oxadiazolo<3,4-c>pyridine

: 225795-65-3
12-chloro-7-(p-chlorophenyl)-10-oxo-indeno<1,2-b>-1,2,5-oxadiazolo<3,4-d>pyridine

Guidance literature:: With PPA; at 125 - 135 ℃; for 24h;
DOI:10.3987/COM-98-S(H)88

Reference yield:

: 21443-48-1
3,4-bis(4'-chlorobenzoyl)-1,2,5-oxadiazole-2-oxide

: 225795-65-3
12-chloro-7-(p-chlorophenyl)-10-oxo-indeno<1,2-b>-1,2,5-oxadiazolo<3,4-d>pyridine

Guidance literature:: Multi-step reaction with 3 steps

1: 37 percent / Zn, glacial acetic acid, acetic anhydride / tetrahydrofuran / 3.5 h / Ambient temperature

2: 84 percent / butan-1-ol / 24 h / Heating

3: 2 percent / polyphosphoric acid / 24 h / 125 - 135 °C

With PPA; acetic anhydride; acetic acid; zinc; In tetrahydrofuran; butan-1-ol;
DOI:10.3987/COM-98-S(H)88

Reference yield:

: 99-91-2
para-chloroacetophenone

: 225795-65-3
12-chloro-7-(p-chlorophenyl)-10-oxo-indeno<1,2-b>-1,2,5-oxadiazolo<3,4-d>pyridine

Guidance literature:: Multi-step reaction with 4 steps

1: HNO₃, NaNO₂

2: 37 percent / Zn, glacial acetic acid, acetic anhydride / tetrahydrofuran / 3.5 h / Ambient temperature

3: 84 percent / butan-1-ol / 24 h / Heating

4: 2 percent / polyphosphoric acid / 24 h / 125 - 135 °C

With PPA; nitric acid; acetic anhydride; acetic acid; zinc; sodium nitrite; In tetrahydrofuran; butan-1-ol;
DOI:10.3987/COM-98-S(H)88