5-{2-[Benzyl-(2-hydroxy-4-o-tolyl-butyl)-amino]-ethoxy}-2-hydroxy-benzamide

Base Information

Chemical Name:5-{2-[Benzyl-(2-hydroxy-4-o-tolyl-butyl)-amino]-ethoxy}-2-hydroxy-benzamide
CAS No.:79407-28-6
Molecular Formula:C₂₇H₃₂N₂O₄
Molecular Weight:448.562
Hs Code.:

Synonyms:5-{2-[Benzyl-(2-hydroxy-4-o-tolyl-butyl)-amino]-ethoxy}-2-hydroxy-benzamide

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Chemical Property of 5-{2-[Benzyl-(2-hydroxy-4-o-tolyl-butyl)-amino]-ethoxy}-2-hydroxy-benzamide

Chemical Property:

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Technology Process of 5-{2-[Benzyl-(2-hydroxy-4-o-tolyl-butyl)-amino]-ethoxy}-2-hydroxy-benzamide

There total 6 articles about 5-{2-[Benzyl-(2-hydroxy-4-o-tolyl-butyl)-amino]-ethoxy}-2-hydroxy-benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 52405-73-9
gentisamide

: 79407-28-6
5-{2-[Benzyl-(2-hydroxy-4-o-tolyl-butyl)-amino]-ethoxy}-2-hydroxy-benzamide

Guidance literature:: Multi-step reaction with 4 steps

1: 87 percent / 4-toluenesulfonic acid / 5 h / Heating

2: 82 percent / K₂CO₃ / 14 h / Heating

3: H₂O / 1 h / Heating

4: propan-2-ol / Heating

With potassium carbonate; toluene-4-sulfonic acid; In water; isopropyl alcohol;
DOI:10.1021/jm00373a003

Reference yield:

: 56812-61-4
2-methylbenzylmagnesium bromide

: 79407-28-6
5-{2-[Benzyl-(2-hydroxy-4-o-tolyl-butyl)-amino]-ethoxy}-2-hydroxy-benzamide

Guidance literature:: Multi-step reaction with 3 steps

1: diethyl ether; benzene / 2 h / Heating

2: tetrabutylammonium sulfate, 4 N NaOH / CH₂Cl₂ / 10 h

3: propan-2-ol / Heating

With sodium hydroxide; tetrabutylammonium sulfate; In diethyl ether; dichloromethane; isopropyl alcohol; benzene;
DOI:10.1021/jm00373a003

Reference yield:

: 79407-26-4
1-chloro-4-(2-methylphenyl)-2-butanol

: 79407-28-6
5-{2-[Benzyl-(2-hydroxy-4-o-tolyl-butyl)-amino]-ethoxy}-2-hydroxy-benzamide

Guidance literature:: Multi-step reaction with 2 steps

1: tetrabutylammonium sulfate, 4 N NaOH / CH₂Cl₂ / 10 h

2: propan-2-ol / Heating

With sodium hydroxide; tetrabutylammonium sulfate; In dichloromethane; isopropyl alcohol;
DOI:10.1021/jm00373a003