(S)-2-((benzyloxycarbonyl)amino)-3-O-(2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)propanoate

Base Information

Chemical Name:(S)-2-((benzyloxycarbonyl)amino)-3-O-(2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)propanoate
CAS No.:77870-90-7
Molecular Formula:C₄₆H₄₉NO₁₀
Molecular Weight:775.896
Hs Code.:

Synonyms:(S)-2-((benzyloxycarbonyl)amino)-3-O-(2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)propanoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-2-((benzyloxycarbonyl)amino)-3-O-(2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)propanoate

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Technology Process of (S)-2-((benzyloxycarbonyl)amino)-3-O-(2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)propanoate

There total 16 articles about (S)-2-((benzyloxycarbonyl)amino)-3-O-(2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 31.5%

: 4291-69-4,6386-24-9,6564-72-3,59531-24-7,69257-52-9,78184-89-1,78609-16-2,78609-17-3,78609-18-4,96553-53-6,104111-61-7,131347-08-5,4132-28-9
2,3,4,6-Tetra-O-benzyl-D-glucopyranose

: 1676-81-9
N-benzyloxycarbonyl-L-serine methyl ester

: 77870-91-8
(S)-2-((benzyloxycarbonyl)amino)-3-O-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)propanoate

: 77870-90-7
(S)-2-((benzyloxycarbonyl)amino)-3-O-(2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)propanoate

Guidance literature:: With trifluoromethanesulfonic acid anhydride; In dichloromethane; -70 degC, 5 min; 15 min, r.t.;

Reference yield:

: 1676-81-9
N-benzyloxycarbonyl-L-serine methyl ester

: 329365-86-8
ethyl 2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl disulfide

: 77870-91-8
(S)-2-((benzyloxycarbonyl)amino)-3-O-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)propanoate

: 77870-90-7
(S)-2-((benzyloxycarbonyl)amino)-3-O-(2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)propanoate

Guidance literature:: With 4 A molecular sieve; dimethyl-(methylthio)-sulphonium trifluoromethanesulphonate; In dichloromethane; at 20 ℃; for 1.5h;
DOI:10.1021/jo051374j

Reference yield:

: 1676-81-9
N-benzyloxycarbonyl-L-serine methyl ester

: Diphenyl-phosphinic acid (3R,4S,5R,6R)-3,4,5-tris-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-2-yl ester

: 77870-91-8
(S)-2-((benzyloxycarbonyl)amino)-3-O-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)propanoate

: 77870-90-7
(S)-2-((benzyloxycarbonyl)amino)-3-O-(2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)propanoate

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; at -78 ℃; for 0.416667h; Yield given. Yields of byproduct given;
DOI:10.1039/a805206i