benzyl 2-(benzyloxy)-4-(N-(4-cyclohexylbenzyl)-2-((4-methylphenyl)sulfonamido)acetamido)benzoate

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Chemical Name:benzyl 2-(benzyloxy)-4-(N-(4-cyclohexylbenzyl)-2-((4-methylphenyl)sulfonamido)acetamido)benzoate
CAS No.:1331747-40-0
Molecular Formula:C₄₃H₄₄N₂O₆S
Molecular Weight:716.898
Hs Code.:

Synonyms:benzyl 2-(benzyloxy)-4-(N-(4-cyclohexylbenzyl)-2-((4-methylphenyl)sulfonamido)acetamido)benzoate

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Chemical Property of benzyl 2-(benzyloxy)-4-(N-(4-cyclohexylbenzyl)-2-((4-methylphenyl)sulfonamido)acetamido)benzoate

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Technology Process of benzyl 2-(benzyloxy)-4-(N-(4-cyclohexylbenzyl)-2-((4-methylphenyl)sulfonamido)acetamido)benzoate

There total 10 articles about benzyl 2-(benzyloxy)-4-(N-(4-cyclohexylbenzyl)-2-((4-methylphenyl)sulfonamido)acetamido)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 1241833-16-8
benzyl 2-(benzyloxy)-4-((4-cyclohexylbenzyl)amino)benzoate

: 1080-44-0
N-Tosylglycine

: 1331747-40-0
benzyl 2-(benzyloxy)-4-(N-(4-cyclohexylbenzyl)-2-((4-methylphenyl)sulfonamido)acetamido)benzoate

Guidance literature:: N-Tosylglycine; With dichlorotriphenylphosphorane; In chloroform; at 20 ℃; for 0.25h;

benzyl 2-(benzyloxy)-4-((4-cyclohexylbenzyl)amino)benzoate; In chloroform; at 100 ℃; for 0.5h; Irradiation;
DOI:10.1021/acsmedchemlett.5b00171

Reference yield: 48.0%

: 1241833-16-8
benzyl 2-(benzyloxy)-4-((4-cyclohexylbenzyl)amino)benzoate

: methyl 2-(N-(tert-butoxycarbonyl)-4-methylphenylsulfonamido)acetic acid

: 1331747-40-0
benzyl 2-(benzyloxy)-4-(N-(4-cyclohexylbenzyl)-2-((4-methylphenyl)sulfonamido)acetamido)benzoate

Guidance literature:: With dichlorotriphenylphosphorane; In chloroform; at 60 ℃; for 12h; Inert atmosphere;
DOI:10.1002/cmdc.201100194

Reference yield:

: 1241832-99-4
benzyl 4-amino-2-(benzyloxy)benzoate

: 1331747-40-0
benzyl 2-(benzyloxy)-4-(N-(4-cyclohexylbenzyl)-2-((4-methylphenyl)sulfonamido)acetamido)benzoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: acetic acid / methanol / 3 h / 45 °C / Molecular sieve; Inert atmosphere

1.2: 12 h / 20 °C / Inert atmosphere

2.1: dichlorotriphenylphosphorane / chloroform / 12 h / 60 °C / Inert atmosphere

With acetic acid; dichlorotriphenylphosphorane; In methanol; chloroform;
DOI:10.1002/cmdc.201100194