(2R,3R)-3-hydroxy-1,4-dimethoxy-1,1,4,4-tetraphenylbutan-2-yl 4-methoxybenzoate

Base Information

• Chemical Name: (2R,3R)-3-hydroxy-1,4-dimethoxy-1,1,4,4-tetraphenylbutan-2-yl 4-methoxybenzoate
• CAS No.: 130874-92-9
• Molecular Formula: C₃₈H₃₆O₆
• Molecular Weight: 588.7
• Mol file: 130874-92-9.mol

Synonyms:(2R,3R)-3-hydroxy-1,4-dimethoxy-1,1,4,4-tetraphenylbutan-2-yl 4-methoxybenzoate

Chemical Property of (2R,3R)-3-hydroxy-1,4-dimethoxy-1,1,4,4-tetraphenylbutan-2-yl 4-methoxybenzoate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (2R,3R)-3-hydroxy-1,4-dimethoxy-1,1,4,4-tetraphenylbutan-2-yl 4-methoxybenzoate

There total 1 articles about (2R,3R)-3-hydroxy-1,4-dimethoxy-1,1,4,4-tetraphenylbutan-2-yl 4-methoxybenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

(4R,5R)-4,5-bis(methoxymethyl)-2-(p-methoxyphenyl)-α,α,α',α'-tetraphenyl-1,3-dioxolane (130888-43-6) → (2R,3R)-3-hydroxy-1,4-dimethoxy-1,1,4,4-tetraphenylbutan-2-yl 4-methoxybenzoate (130874-92-9)

Guidance literature:

With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane; water; for 1.5h;

DOI:10.1016/S0040-4020(01)86753-3

Reference yield: 80.0%

(2R,3R)-3-hydroxy-1,4-dimethoxy-1,1,4,4-tetraphenylbutan-2-yl 4-methoxybenzoate (130874-92-9) → (2R,3R)-1,4-dimethoxy-1,1,4,4-tetraphenyl-2,3-butandiol (130874-89-4)

Guidance literature:

With lithium aluminium tetrahydride; In diethyl ether; for 2h; Ambient temperature;

DOI:10.1016/S0040-4020(01)86753-3

upstream raw materials:

(4R,5R)-4,5-bis(methoxymethyl)-2-(p-methoxyphenyl)-α,α,α',α'-tetraphenyl-1,3-dioxolane

Downstream raw materials:

(2R,3R)-1,4-dimethoxy-1,1,4,4-tetraphenyl-2,3-butandiol