4-methoxyphenyl 3-O-acetyl-4,6-di-O-benzoyl-2-O-(2,3,4-tri-O-benzoyl-6-methyl-β-D-glucopyranuronosyl)-α-D-mannopyranoside

Base Information

Chemical Name:4-methoxyphenyl 3-O-acetyl-4,6-di-O-benzoyl-2-O-(2,3,4-tri-O-benzoyl-6-methyl-β-D-glucopyranuronosyl)-α-D-mannopyranoside
CAS No.:1423987-41-0
Molecular Formula:C₅₇H₅₀O₁₉
Molecular Weight:1039.01
Hs Code.:

Synonyms:4-methoxyphenyl 3-O-acetyl-4,6-di-O-benzoyl-2-O-(2,3,4-tri-O-benzoyl-6-methyl-β-D-glucopyranuronosyl)-α-D-mannopyranoside

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Chemical Property of 4-methoxyphenyl 3-O-acetyl-4,6-di-O-benzoyl-2-O-(2,3,4-tri-O-benzoyl-6-methyl-β-D-glucopyranuronosyl)-α-D-mannopyranoside

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Technology Process of 4-methoxyphenyl 3-O-acetyl-4,6-di-O-benzoyl-2-O-(2,3,4-tri-O-benzoyl-6-methyl-β-D-glucopyranuronosyl)-α-D-mannopyranoside

There total 11 articles about 4-methoxyphenyl 3-O-acetyl-4,6-di-O-benzoyl-2-O-(2,3,4-tri-O-benzoyl-6-methyl-β-D-glucopyranuronosyl)-α-D-mannopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1423987-49-8
4-methoxyphenyl 3-O-acetyl-4,6-di-O-benzoyl-α-D-mannopyranoside

: methyl 2,3,4-tri-O-benzoyl-1-O-trichloroacetimidoyl-α-D-glucopyranuronate

: 1423987-41-0
4-methoxyphenyl 3-O-acetyl-4,6-di-O-benzoyl-2-O-(2,3,4-tri-O-benzoyl-6-methyl-β-D-glucopyranuronosyl)-α-D-mannopyranoside

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at -30 - 20 ℃; for 3h; Inert atmosphere;
DOI:10.1002/hlca.201400297

Reference yield:

: 1423987-79-4
N,O-dimethyl-N-(2,3,4-tri-O-benzoyl-β-D-glucopyranuronic acid)

: 1423987-41-0
4-methoxyphenyl 3-O-acetyl-4,6-di-O-benzoyl-2-O-(2,3,4-tri-O-benzoyl-6-methyl-β-D-glucopyranuronosyl)-α-D-mannopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1.1: chloro-trimethyl-silane / tetrahydrofuran / 2 h / 20 °C / Inert atmosphere

2.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane / 1 h / 0 °C / Inert atmosphere

3.1: dichloromethane / 1 h / 20 °C / Molecular sieve

3.2: 0.5 h / -20 °C / Inert atmosphere

With chloro-trimethyl-silane; 1,8-diazabicyclo[5.4.0]undec-7-ene; In tetrahydrofuran; dichloromethane;
DOI:10.1080/07328303.2012.762104

Reference yield:

: C₂₇H₂₂O₁₀

: 1423987-41-0
4-methoxyphenyl 3-O-acetyl-4,6-di-O-benzoyl-2-O-(2,3,4-tri-O-benzoyl-6-methyl-β-D-glucopyranuronosyl)-α-D-mannopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium acetate / water / 20 h / 0 - 20 °C

2.1: chloro-trimethyl-silane / tetrahydrofuran / 2 h / 20 °C / Inert atmosphere

3.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane / 1 h / 0 °C / Inert atmosphere

4.1: dichloromethane / 1 h / 20 °C / Molecular sieve

4.2: 0.5 h / -20 °C / Inert atmosphere

With chloro-trimethyl-silane; sodium acetate; 1,8-diazabicyclo[5.4.0]undec-7-ene; In tetrahydrofuran; dichloromethane; water;
DOI:10.1080/07328303.2012.762104