Technology Process of C19H30O4
There total 13 articles about C19H30O4 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
C19H28O2;
With
methanesulfonamide; AD-mix-β;
In
water; tert-butyl alcohol;
at 0 - 20 ℃;
for 16h;
With
potassium carbonate;
In
methanol;
at 0 ℃;
for 4h;
DOI:10.1021/ol1028699
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: ammonium molibdate; dihydrogen peroxide / ethanol / 21 h / 0 °C
2.1: sodium hexamethyldisilazane / 1,2-dimethoxyethane; toluene / 0.08 h / -78 °C
2.2: 1 h / -50 °C
3.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 16 h / 0 - 20 °C
4.1: sodium hydride / tetrahydrofuran; mineral oil / 1 h / 0 - 20 °C
4.2: 2 h / 0 - 20 °C
5.1: AD-mix-β; methanesulfonamide / water; tert-butyl alcohol / 16 h / 0 - 20 °C
5.2: 4 h / 0 °C
With
ammonium molibdate; methanesulfonamide; AD-mix-β; tetrabutyl ammonium fluoride; dihydrogen peroxide; sodium hexamethyldisilazane; sodium hydride;
In
tetrahydrofuran; 1,2-dimethoxyethane; ethanol; water; toluene; mineral oil; tert-butyl alcohol;
2.1: Julia Olefin synthesis / 2.2: Julia Olefin synthesis;
DOI:10.1021/ol1028699
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: sodium hexamethyldisilazane / 1,2-dimethoxyethane; toluene / 0.08 h / -78 °C
1.2: 1 h / -50 °C
2.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 16 h / 0 - 20 °C
3.1: sodium hydride / tetrahydrofuran; mineral oil / 1 h / 0 - 20 °C
3.2: 2 h / 0 - 20 °C
4.1: AD-mix-β; methanesulfonamide / water; tert-butyl alcohol / 16 h / 0 - 20 °C
4.2: 4 h / 0 °C
With
methanesulfonamide; AD-mix-β; tetrabutyl ammonium fluoride; sodium hexamethyldisilazane; sodium hydride;
In
tetrahydrofuran; 1,2-dimethoxyethane; water; toluene; mineral oil; tert-butyl alcohol;
1.1: Julia Olefin synthesis / 1.2: Julia Olefin synthesis;
DOI:10.1021/ol1028699
