Technology Process of 9-(4-methoxy-benzyloxy)-nonanal
There total 5 articles about 9-(4-methoxy-benzyloxy)-nonanal which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
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Multi-step reaction with 2 steps
1.1: sodium hydride / tetrahydrofuran; dimethyl sulfoxide; mineral oil / 1 h / 0 °C
1.2: 18.5 h / 0 - 20 °C
2.1: Dess-Martin periodane / dichloromethane / 20 °C / Cooling with ice
With
sodium hydride; Dess-Martin periodane;
In
tetrahydrofuran; dichloromethane; dimethyl sulfoxide; mineral oil;
DOI:10.1021/ol3017676
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 95 percent / NaH; tetra(n-butyl)ammonium iodide / dimethylformamide / 1 h / 0 °C
2: (COCl)2; Et3N; DMSO / CH2Cl2 / -60 - 20 °C
With
oxalyl dichloride; tetra-(n-butyl)ammonium iodide; sodium hydride; dimethyl sulfoxide; triethylamine;
In
dichloromethane; N,N-dimethyl-formamide;
2: Swern oxidation;
DOI:10.1016/j.tet.2007.05.047
