C₂₂H₂₉N₃O₇S

Base Information

Chemical Name:C₂₂H₂₉N₃O₇S
CAS No.:1449016-74-3
Molecular Formula:C₂₂H₂₉N₃O₇S
Molecular Weight:479.554
Hs Code.:

C<sub>22</sub>H<sub>29</sub>N<sub>3</sub>O<sub>7</sub>S

Synonyms:C₂₂H₂₉N₃O₇S

Suppliers and Price of C₂₂H₂₉N₃O₇S

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₂₂H₂₉N₃O₇S

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₂₂H₂₉N₃O₇S

There total 7 articles about C₂₂H₂₉N₃O₇S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1449016-68-5
C₂₂H₂₇N₃O₇S

: 1449016-74-3
C₂₂H₂₉N₃O₇S

Guidance literature:: With diisobutylaluminium hydride; In tetrahydrofuran; toluene; at -78 - 20 ℃; for 0.75h;
DOI:10.1002/ejoc.201201516

Reference yield:

: 60410-16-4
(1R,4S)-4-hydroxy-2-cyclopentene-1-yl acetate

: 1449016-74-3
C₂₂H₂₉N₃O₇S

Guidance literature:: Multi-step reaction with 8 steps

1.1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 18 h / 0 - 20 °C

2.1: potassium carbonate; thiophenol / tetrahydrofuran; N,N-dimethyl-formamide / 3.5 h / 20 - 70 °C

2.2: 12 h / 60 °C

2.3: 12 h / 20 °C

3.1: potassium hydride; dibenzo-18-crown-6 / tetrahydrofuran / 20 °C

4.1: n-butyllithium / tetrahydrofuran / 17.5 h / -100 - -60 °C

5.1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 20 h / 0 °C

6.1: Hoveyda-Grubbs catalyst second generation; ethene / dichloromethane / 24 h / -10 - 45 °C / 760.05 Torr / Inert atmosphere

7.1: sodium periodate; silica gel / acetonitrile; ethyl acetate / 24 h / 20 °C

8.1: diisobutylaluminium hydride / tetrahydrofuran; toluene / 0.75 h / -78 - 20 °C

With sodium periodate; dibenzo-18-crown-6; n-butyllithium; Hoveyda-Grubbs catalyst second generation; ethene; di-isopropyl azodicarboxylate; silica gel; potassium hydride; diisobutylaluminium hydride; potassium carbonate; thiophenol; triphenylphosphine; In tetrahydrofuran; dichloromethane; ethyl acetate; N,N-dimethyl-formamide; toluene; acetonitrile; 1.1: |Fukuyama Coupling / 3.1: |Williamson Ether Synthesis / 4.1: |Wittig Rearrangement / 5.1: |Fukuyama Coupling;
DOI:10.1002/ejoc.201201516

Reference yield:

: allyl-((1R,4R)-4-tributylstannanylmethoxy-cyclopent-2-enyl)-carbamic acid tert-butyl ester

: 1449016-74-3
C₂₂H₂₉N₃O₇S

Guidance literature:: Multi-step reaction with 5 steps

1: n-butyllithium / tetrahydrofuran / 17.5 h / -100 - -60 °C

2: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 20 h / 0 °C

3: Hoveyda-Grubbs catalyst second generation; ethene / dichloromethane / 24 h / -10 - 45 °C / 760.05 Torr / Inert atmosphere

4: sodium periodate; silica gel / acetonitrile; ethyl acetate / 24 h / 20 °C

5: diisobutylaluminium hydride / tetrahydrofuran; toluene / 0.75 h / -78 - 20 °C

With sodium periodate; n-butyllithium; Hoveyda-Grubbs catalyst second generation; ethene; di-isopropyl azodicarboxylate; silica gel; diisobutylaluminium hydride; triphenylphosphine; In tetrahydrofuran; dichloromethane; ethyl acetate; toluene; acetonitrile; 1: |Wittig Rearrangement / 2: |Fukuyama Coupling;
DOI:10.1002/ejoc.201201516