Allyl O-<3,4-isopropylidene-2-O-(4-methoxybenzyl)-α-L-fucopyranosyl>-(1->6)-2-acetamido-2-deoxy-3,4-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)-β-D-glucopyranoside

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Chemical Name:Allyl O-<3,4-isopropylidene-2-O-(4-methoxybenzyl)-α-L-fucopyranosyl>-(1->6)-2-acetamido-2-deoxy-3,4-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)-β-D-glucopyranoside
CAS No.:152015-43-5
Molecular Formula:C₄₀H₆₇NO₁₂Si₂
Molecular Weight:810.142
Hs Code.:

Allyl O-<3,4-isopropylidene-2-O-(4-methoxybenzyl)-α-L-fucopyranosyl>-(1->6)-2-acetamido-2-deoxy-3,4-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)-β-D-glucopyranoside

Synonyms:Allyl O-<3,4-isopropylidene-2-O-(4-methoxybenzyl)-α-L-fucopyranosyl>-(1->6)-2-acetamido-2-deoxy-3,4-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)-β-D-glucopyranoside

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Chemical Property of Allyl O-<3,4-isopropylidene-2-O-(4-methoxybenzyl)-α-L-fucopyranosyl>-(1->6)-2-acetamido-2-deoxy-3,4-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)-β-D-glucopyranoside

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Technology Process of Allyl O-<3,4-isopropylidene-2-O-(4-methoxybenzyl)-α-L-fucopyranosyl>-(1->6)-2-acetamido-2-deoxy-3,4-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)-β-D-glucopyranoside

There total 1 articles about Allyl O-<3,4-isopropylidene-2-O-(4-methoxybenzyl)-α-L-fucopyranosyl>-(1->6)-2-acetamido-2-deoxy-3,4-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 20.0%

: 131338-01-7
allyl 2-acetamido-2-deoxy-3,4-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)-β-D-glucopyranoside

: 152015-42-4
S-ethyl 3,4-O-isopropylidene-2-O-p-methoxybenzyl-1-thio-β-L-fucopyranoside

: 152015-43-5
Allyl O-<3,4-isopropylidene-2-O-(4-methoxybenzyl)-α-L-fucopyranosyl>-(1->6)-2-acetamido-2-deoxy-3,4-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)-β-D-glucopyranoside

: Allyl O-<3,4-isopropylidene-2-O-(4-methoxybenzyl)-β-L-fucopyranosyl>-(1->6)-2-acetamido-2-deoxy-3,4-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)-β-D-glucopyranoside

Guidance literature:: With iodonium(di-γ-collidine) perchlorate; 4 A molecular sieve; In diethyl ether; dichloromethane; for 20h; Ambient temperature;
DOI:10.1016/0008-6215(93)84047-A

Reference yield: 82.0%

: 152015-43-5
Allyl O-<3,4-isopropylidene-2-O-(4-methoxybenzyl)-α-L-fucopyranosyl>-(1->6)-2-acetamido-2-deoxy-3,4-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)-β-D-glucopyranoside

: 152015-44-6
Allyl O-<3,4-isopropylidene-2-O-(4-methoxybenzyl)-α-L-fucopyranosyl>-(1->6)-2-acetamido-2-deoxy-β-D-glucopyranoside

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; for 4h; Ambient temperature;
DOI:10.1016/0008-6215(93)84047-A

Reference yield:

: 152015-43-5
Allyl O-<3,4-isopropylidene-2-O-(4-methoxybenzyl)-α-L-fucopyranosyl>-(1->6)-2-acetamido-2-deoxy-3,4-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)-β-D-glucopyranoside

: Allyl 2-acetamido-2-deoxy-3,6-di-O-<3,4-O-isopropylidene-2-O-(4-methoxybenzyl)-α-L-fucopyranosyl>-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 82 percent / Bu₄NF / tetrahydrofuran / 4 h / Ambient temperature

2: 27 percent / iodonium di-sym-collidinium perchlorate (IDCP), molecular sieves (4 Angstroem) / CH₂Cl₂; diethyl ether / 3 h / Ambient temperature

With iodonium(di-γ-collidine) perchlorate; 4 A molecular sieve; tetrabutyl ammonium fluoride; In tetrahydrofuran; diethyl ether; dichloromethane;
DOI:10.1016/0008-6215(93)84047-A