(N,N'-diisopropylphenyl-2,4-pentanediimine)Yb(THF)(2,6-di-tert-butyl-4-methylphenoxo)*THF

Base Information

Chemical Name:(N,N'-diisopropylphenyl-2,4-pentanediimine)Yb(THF)(2,6-di-tert-butyl-4-methylphenoxo)*THF
CAS No.:573984-29-9
Molecular Formula:C₄H₈O*C₄₈H₇₂N₂O₂Yb
Molecular Weight:954.259
Hs Code.:

Synonyms:(N,N'-diisopropylphenyl-2,4-pentanediimine)Yb(THF)(2,6-di-tert-butyl-4-methylphenoxo)*THF

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Chemical Property of (N,N'-diisopropylphenyl-2,4-pentanediimine)Yb(THF)(2,6-di-tert-butyl-4-methylphenoxo)*THF

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Technology Process of (N,N'-diisopropylphenyl-2,4-pentanediimine)Yb(THF)(2,6-di-tert-butyl-4-methylphenoxo)*THF

There total 2 articles about (N,N'-diisopropylphenyl-2,4-pentanediimine)Yb(THF)(2,6-di-tert-butyl-4-methylphenoxo)*THF which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.1%

: 109-99-9,24979-97-3,77392-70-2
tetrahydrofuran

: 573984-25-5
(N,N'-diisopropylphenyl-2,4-pentanediimine)YbCl(THF)(2,6-di-tert-butyl-4-methylphenoxo)

: 573984-29-9
(N,N'-diisopropylphenyl-2,4-pentanediimine)Yb(THF)(2,6-di-tert-butyl-4-methylphenoxo)*THF

Guidance literature:: With Na/K alloy; In tetrahydrofuran; under Ar atm. using Schlenk techniques; to THF soln. of Yb complex addedNa/K alloy; mixt. stirred at room temp. for 48 h; ppt. removed by centrifugation; THF removed (vac.); toluene added; ppt. removed by centrifugation; crystals were obtained from concd. toluene soln. at -20°C for a 3 ds; elem. anal.;
DOI:10.1021/om030136g

Reference yield:

: (2-((2,6-diisopropylphenyl)amino)-4-((2,6-diisopropylphenyl)imino)-pent-2-ene) lithium salt

: 16654-89-0
sodium 2,6-di-tert-butyl-4-methylphenoxide

: 573984-29-9
(N,N'-diisopropylphenyl-2,4-pentanediimine)Yb(THF)(2,6-di-tert-butyl-4-methylphenoxo)*THF

Guidance literature:: Multi-step reaction with 2 steps

1: toluene; tetrahydrofuran; hexane

2: Na/K alloy / tetrahydrofuran

With Na/K alloy; In tetrahydrofuran; hexane; toluene;
DOI:10.1021/om030136g