C₂₅H₂₁ClN₂O₅

Base Information

Chemical Name:C₂₅H₂₁ClN₂O₅
CAS No.:1423684-81-4
Molecular Formula:C₂₅H₂₁ClN₂O₅
Molecular Weight:464.905
Hs Code.:

C<sub>25</sub>H<sub>21</sub>ClN<sub>2</sub>O<sub>5</sub>

Synonyms:C₂₅H₂₁ClN₂O₅

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Chemical Property of C₂₅H₂₁ClN₂O₅

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Technology Process of C₂₅H₂₁ClN₂O₅

There total 9 articles about C₂₅H₂₁ClN₂O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 14.2%

: 1423690-66-7
C₂₇H₂₅ClN₂O₅

: 1423684-81-4
C₂₅H₂₁ClN₂O₅

Guidance literature:: C₂₇H₂₅ClN₂O₅; With water; lithium hydroxide; In methanol; at 60 ℃; Inert atmosphere;

In water; Acidic conditions;

Reference yield:

: 2142-68-9
1-(2-chlorophenyl)ethanone

: 1423684-81-4
C₂₅H₂₁ClN₂O₅

Guidance literature:: Multi-step reaction with 3 steps

1.1: (S)-tetrahydro-1-butyl-3,3-diphenyl-1H,3H-pyrrolo{2,1-c}{1,3,2}oxazaborole; dimethylsulfide borane complex / tetrahydrofuran / 0.5 h / 20 °C

2.1: pyridine / 1,2-dichloro-ethane / 1 h / 0 - 20 °C / Inert atmosphere

2.2: 80 °C / Inert atmosphere

3.1: lithium hydroxide; water / methanol / 60 °C / Inert atmosphere

3.2: Acidic conditions

With pyridine; dimethylsulfide borane complex; water; lithium hydroxide; (S)-tetrahydro-1-butyl-3,3-diphenyl-1H,3H-pyrrolo{2,1-c}{1,3,2}oxazaborole; In tetrahydrofuran; methanol; 1,2-dichloro-ethane;

Reference yield:

: 909389-74-8
acetic acid 3,5-dibromo-phenyl ester

: 1423684-81-4
C₂₅H₂₁ClN₂O₅

Guidance literature:: Multi-step reaction with 10 steps

1.1: aluminum (III) chloride / 3 h / 160 °C / Inert atmosphere

2.1: sodium carbonate / N,N-dimethyl-formamide / 0 - 20 °C / Inert atmosphere

3.1: pyridine; hydroxylamine hydrochloride / 6 h / 130 °C / Inert atmosphere

4.1: N,N`-dimethylethylenediamine; sodium t-butanolate; copper(l) iodide / tetrahydrofuran / 1 h / 20 °C / Inert atmosphere

5.1: boron tribromide / dichloromethane / 0 °C / Inert atmosphere

6.1: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; sodium carbonate / water; 1,2-dimethoxyethane / 80 °C / Inert atmosphere

7.1: triethylamine / dichloromethane / 0 - 20 °C / Inert atmosphere

8.1: palladium diacetate; caesium carbonate; Benzophenone imine; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene / tetrahydrofuran / 80 °C / Inert atmosphere

9.1: pyridine / 1,2-dichloro-ethane / 1 h / 0 - 20 °C / Inert atmosphere

9.2: 80 °C / Inert atmosphere

10.1: lithium hydroxide; water / methanol / 60 °C / Inert atmosphere

10.2: Acidic conditions

With pyridine; Benzophenone imine; aluminum (III) chloride; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; copper(l) iodide; hydroxylamine hydrochloride; water; palladium diacetate; boron tribromide; sodium carbonate; caesium carbonate; triethylamine; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; lithium hydroxide; sodium t-butanolate; N,N`-dimethylethylenediamine; In tetrahydrofuran; methanol; 1,2-dimethoxyethane; dichloromethane; water; 1,2-dichloro-ethane; N,N-dimethyl-formamide;