N,N-dibenzyl-1-((1S,4R)-7,7-dimethyl-2-oxobicyclo[2.2.1]heptan-1-yl)methanesulfonamide

Base Information

• Chemical Name: N,N-dibenzyl-1-((1S,4R)-7,7-dimethyl-2-oxobicyclo[2.2.1]heptan-1-yl)methanesulfonamide
• CAS No.: 156730-39-1
• Molecular Formula: C₂₄H₂₉NO₃S
• Molecular Weight: 411.565

Synonyms:N,N-dibenzyl-1-((1S,4R)-7,7-dimethyl-2-oxobicyclo[2.2.1]heptan-1-yl)methanesulfonamide

Chemical Property of N,N-dibenzyl-1-((1S,4R)-7,7-dimethyl-2-oxobicyclo[2.2.1]heptan-1-yl)methanesulfonamide

Chemical Property:

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Technology Process of N,N-dibenzyl-1-((1S,4R)-7,7-dimethyl-2-oxobicyclo[2.2.1]heptan-1-yl)methanesulfonamide

There total 2 articles about N,N-dibenzyl-1-((1S,4R)-7,7-dimethyl-2-oxobicyclo[2.2.1]heptan-1-yl)methanesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

((1S,4R)-7,7-dimethyl-2-oxobicyclo[2.2.1]heptan-1-yl)methanesulfonyl fluoride + dibenzylamine (103-49-1) → N,N-dibenzyl-1-((1S,4R)-7,7-dimethyl-2-oxobicyclo[2.2.1]heptan-1-yl)methanesulfonamide (156730-39-1,616214-72-3)

Guidance literature:

With 1,1,3,3-Tetramethyldisiloxane; benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine; In dimethyl sulfoxide; at 25 ℃; for 48h; Sealed tube;

DOI:10.1002/anie.202013976

Reference yield: 78.0%

Camphorsulfonyl chloride (21286-54-4) + dibenzylamine (103-49-1) → N,N-dibenzyl-1-((1S,4R)-7,7-dimethyl-2-oxobicyclo[2.2.1]heptan-1-yl)methanesulfonamide (156730-39-1,616214-72-3)

Guidance literature:

With isoquinoline; dmap; In N,N-dimethyl-formamide; at 0 ℃; for 1h;

DOI:10.1021/jo00094a013

Reference yield: 92.0%

N,N-dibenzyl-1-((1S,4R)-7,7-dimethyl-2-oxobicyclo[2.2.1]heptan-1-yl)methanesulfonamide (156730-39-1,616214-72-3) → (+)-10-<(Dibenzylamino)sulfonyl>bornan-6-ol (156730-37-9)

Guidance literature:

With L-Selectride; In tetrahydrofuran; 1.) -78 deg C, 30 min, 2.) r.t., 4.5 h;

DOI:10.1021/jo00094a013

upstream raw materials:

Camphorsulfonyl chloride

dibenzylamine

Downstream raw materials:

(+)-10-<(Dibenzylamino)sulfonyl>bornan-6-ol

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