(E)-2-[3,4,5-tris(benzyloxy)phenyl]ethenyl-1,3-oxathiolane

Base Information

Chemical Name:(E)-2-[3,4,5-tris(benzyloxy)phenyl]ethenyl-1,3-oxathiolane
CAS No.:1374304-27-4
Molecular Formula:C₃₂H₃₀O₄S
Molecular Weight:510.654
Hs Code.:

Synonyms:(E)-2-[3,4,5-tris(benzyloxy)phenyl]ethenyl-1,3-oxathiolane

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Chemical Property of (E)-2-[3,4,5-tris(benzyloxy)phenyl]ethenyl-1,3-oxathiolane

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Technology Process of (E)-2-[3,4,5-tris(benzyloxy)phenyl]ethenyl-1,3-oxathiolane

There total 2 articles about (E)-2-[3,4,5-tris(benzyloxy)phenyl]ethenyl-1,3-oxathiolane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1374304-26-3
(E)-3-[3,4,5-tris(benzyloxy)phenyl]prop-2-enal

: 60-24-2
2-hydroxyethanethiol

: 1374304-27-4
(E)-2-[3,4,5-tris(benzyloxy)phenyl]ethenyl-1,3-oxathiolane

Guidance literature:: (E)-3-[3,4,5-tris(benzyloxy)phenyl]prop-2-enal; With hydrogen bromide; acetic acid; In toluene; at 20 ℃; for 1h; Inert atmosphere;

2-hydroxyethanethiol; In toluene; at 0 - 20 ℃; for 2.16667h; Inert atmosphere;
DOI:10.1016/j.tetlet.2012.02.065

Reference yield:

: 332386-68-2
(E)-3-[3,4,5-tris(benzyloxy)phenyl]prop-2-en-1-ol

: 1374304-27-4
(E)-2-[3,4,5-tris(benzyloxy)phenyl]ethenyl-1,3-oxathiolane

Guidance literature:: Multi-step reaction with 2 steps

1.1: manganese(IV) oxide / dichloromethane / 12 h / 20 °C / Inert atmosphere

2.1: hydrogen bromide; acetic acid / toluene / 1 h / 20 °C / Inert atmosphere

2.2: 2.17 h / 0 - 20 °C / Inert atmosphere

With manganese(IV) oxide; hydrogen bromide; acetic acid; In dichloromethane; toluene;
DOI:10.1016/j.tetlet.2012.02.065

Reference yield: 98.0%

: 1374304-27-4
(E)-2-[3,4,5-tris(benzyloxy)phenyl]ethenyl-1,3-oxathiolane

: (E)-2-[3,4,5-tris(benzyloxy)phenyl]ethenyl-1,3-oxathiolane 3-oxide

Guidance literature:: With sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; folinic acid; at 0 ℃; for 8h; Inert atmosphere;
DOI:10.1016/j.tetlet.2012.02.065