(4-methyl)-3-pentenyl (S)-2-[(1,1-dimethylethyl)diphenylsilyl]oxypropanoate

Base Information

Chemical Name:(4-methyl)-3-pentenyl (S)-2-[(1,1-dimethylethyl)diphenylsilyl]oxypropanoate
CAS No.:330944-31-5
Molecular Formula:C₂₅H₃₄O₃Si
Molecular Weight:410.629
Hs Code.:

Synonyms:(4-methyl)-3-pentenyl (S)-2-[(1,1-dimethylethyl)diphenylsilyl]oxypropanoate

Suppliers and Price of (4-methyl)-3-pentenyl (S)-2-[(1,1-dimethylethyl)diphenylsilyl]oxypropanoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (4-methyl)-3-pentenyl (S)-2-[(1,1-dimethylethyl)diphenylsilyl]oxypropanoate

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Technology Process of (4-methyl)-3-pentenyl (S)-2-[(1,1-dimethylethyl)diphenylsilyl]oxypropanoate

There total 5 articles about (4-methyl)-3-pentenyl (S)-2-[(1,1-dimethylethyl)diphenylsilyl]oxypropanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 763-89-3
4-methylpent-3-en-1-ol

: 125941-75-5
(S)-2-[(1,1-dimethylethyl)diphenylsilyl]oxypropanoic acid

: 330944-31-5
(4-methyl)-3-pentenyl (S)-2-[(1,1-dimethylethyl)diphenylsilyl]oxypropanoate

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at 0 ℃;
DOI:10.1016/S0040-4039(00)01933-X

Reference yield:

: 87681-25-2
(2S)-2-<(tert-Butyldiphenylsilyl)oxy>propanoic Acid Methyl Ester

: 330944-31-5
(4-methyl)-3-pentenyl (S)-2-[(1,1-dimethylethyl)diphenylsilyl]oxypropanoate

Guidance literature:: Multi-step reaction with 2 steps

1: 89 percent / LiOH / H₂O; tetrahydrofuran / 0 °C

2: 89 percent / DMAP; DCC / CH₂Cl₂ / 0 - 20 °C

With dmap; lithium hydroxide; dicyclohexyl-carbodiimide; In tetrahydrofuran; dichloromethane; water;
DOI:10.1021/jo001631e

Reference yield:

: 58479-61-1
tert-butylchlorodiphenylsilane

: 330944-31-5
(4-methyl)-3-pentenyl (S)-2-[(1,1-dimethylethyl)diphenylsilyl]oxypropanoate

Guidance literature:: Multi-step reaction with 3 steps

1: 89 percent / imidazole / dimethylformamide

2: 89 percent / LiOH / H₂O; tetrahydrofuran / 0 °C

3: 89 percent / DMAP; DCC / CH₂Cl₂ / 0 - 20 °C

With 1H-imidazole; dmap; lithium hydroxide; dicyclohexyl-carbodiimide; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1021/jo001631e