((C₆F₅)2ClAuSP(C₆H₅)2CH₂P(C₆H₅)2CH₂CO₂CH₃)⁽¹⁺⁾*ClO₄^(1-)={(C₆F₅)2ClAuSP(C₆H₅)2CH₂P(C₆H₅)2CH₂COOCH₃}ClO₄

Base Information

• Chemical Name: ((C₆F₅)2ClAuSP(C₆H₅)2CH₂P(C₆H₅)2CH₂CO₂CH₃)⁽¹⁺⁾*ClO₄^(1-)={(C₆F₅)2ClAuSP(C₆H₅)2CH₂P(C₆H₅)2CH₂COOCH₃}ClO₄
• CAS No.: 110317-13-0
• Molecular Formula: C₄₀H₂₇AuClF₁₀O₂P₂S*ClO₄
• Molecular Weight: 1155.52

Synonyms:((C₆F₅)2ClAuSP(C₆H₅)2CH₂P(C₆H₅)2CH₂CO₂CH₃)⁽¹⁺⁾*ClO₄^(1-)={(C₆F₅)2ClAuSP(C₆H₅)2CH₂P(C₆H₅)2CH₂COOCH₃}ClO₄

Chemical Property of ((C₆F₅)2ClAuSP(C₆H₅)2CH₂P(C₆H₅)2CH₂CO₂CH₃)⁽¹⁺⁾*ClO₄^(1-)={(C₆F₅)2ClAuSP(C₆H₅)2CH₂P(C₆H₅)2CH₂COOCH₃}ClO₄

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Technology Process of ((C₆F₅)2ClAuSP(C₆H₅)2CH₂P(C₆H₅)2CH₂CO₂CH₃)⁽¹⁺⁾*ClO₄^(1-)={(C₆F₅)2ClAuSP(C₆H₅)2CH₂P(C₆H₅)2CH₂COOCH₃}ClO₄

There total 1 articles about ((C₆F₅)2ClAuSP(C₆H₅)2CH₂P(C₆H₅)2CH₂CO₂CH₃)⁽¹⁺⁾*ClO₄^(1-)={(C₆F₅)2ClAuSP(C₆H₅)2CH₂P(C₆H₅)2CH₂COOCH₃}ClO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

[Au(pentafluorophenyl)2Cl]2 + SP(C6H5)2CH2P(C6H5)2CH2COOCH3(1+)*ClO4(1-)=(SP(C6H5)2CH2P(C6H5)2CH2COOCH3)ClO4 (110317-30-1) → ((C6F5)2ClAuSP(C6H5)2CH2P(C6H5)2CH2CO2CH3)(1+)*ClO4(1-)={(C6F5)2ClAuSP(C6H5)2CH2P(C6H5)2CH2COOCH3}ClO4 (110317-13-0)

Guidance literature:

In dichloromethane; addn. of ligand to a suspn. of complex in CH2Cl2; stirring for 3 h at room temp.;; filtered, concd., pptd. by addn. of Et2O; elem. anal.;;

DOI:10.1021/om00154a010

Reference yield: 75.0%

((C6F5)2ClAuSP(C6H5)2CH2P(C6H5)2CH2CO2CH3)(1+)*ClO4(1-)={(C6F5)2ClAuSP(C6H5)2CH2P(C6H5)2CH2COOCH3}ClO4 (110317-13-0) → ((C6F5)2AuSP(C6H5)2CHP(C6H5)2CHCO2CH3) (110317-15-2)

Guidance literature:

With Na₂CO₃; In chloroform; byproducts: NaClO4, NaCl; addn. of Na2CO3 to a soln. of complex in CHCl3; stirring for 2 h at reflux temp.;; filtered under N2, evapd., pptd. by addn. of hexane; elem. anal.;;

DOI:10.1021/om00154a010

Reference yield: 65.0%

((C6F5)2ClAuSP(C6H5)2CH2P(C6H5)2CH2CO2CH3)(1+)*ClO4(1-)={(C6F5)2ClAuSP(C6H5)2CH2P(C6H5)2CH2COOCH3}ClO4 (110317-13-0) + silver perchlorate → ((C6F5)2AuSP(C6H5)2CHP(C6H5)2CH2CO2CH3)(1+)*ClO4(1-)={(C6F5)2AuSP(C6H5)2CHP(C6H5)2CH2COOCH3}ClO4 (110317-19-6)

Guidance literature:

In dichloromethane; addn. of AgClO4 to a soln. of the complex in CH2Cl2; stirring for 8 h at room temp.;; filtered, evapd., Et2O was added; elem. anal.;;

DOI:10.1021/om00154a010

upstream raw materials:

SP(C₆H₅)2CH₂P(C₆H₅)2CH₂COOCH₃⁽¹⁺⁾*ClO₄^(1-)=(SP(C₆H₅)2CH₂P(C₆H₅)2CH₂COOCH₃)ClO₄

Downstream raw materials:

((C₆F₅)2AuSP(C₆H₅)2CHP(C₆H₅)2CHCO₂CH₃)

((C₆F₅)2AuSP(C₆H₅)2CHP(C₆H₅)2CH₂CO₂CH₃)⁽¹⁺⁾*ClO₄^(1-)={(C₆F₅)2AuSP(C₆H₅)2CHP(C₆H₅)2CH₂COOCH₃}ClO₄

((C₆F₅)2AuSP(C₆H₅)2CH(AuC₆F₅)P(C₆H₅)2CHCO₂CH₃)

((C₆F₅)2AuSP(C₆H₅)2CH₂P(C₆H₅)2CHCO₂CH₃)⁽¹⁺⁾*ClO₄^(1-)={(C₆F₅)2AuSP(C₆H₅)2CH₂P(C₆H₅)2CHCOOCH₃}ClO₄

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