C₄₆H₃₃BN₂

Base Information

Chemical Name:C₄₆H₃₃BN₂
CAS No.:1347741-49-4
Molecular Formula:C₄₆H₃₃BN₂
Molecular Weight:624.592
Hs Code.:

C<sub>46</sub>H<sub>33</sub>BN<sub>2</sub>

Synonyms:C₄₆H₃₃BN₂

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Chemical Property of C₄₆H₃₃BN₂

Chemical Property:

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Technology Process of C₄₆H₃₃BN₂

There total 4 articles about C₄₆H₃₃BN₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1347741-61-0
N,N-bis(2-bromophenyl)-N',N'-diphenylbenzene-1,4-diamine

: 612086-25-6
4,4,5,5-tetramethyl-2-(2-phenyl-naphthalen-1-yl)-[1,3,2]dioxaborolane

: 1347741-49-4
C₄₆H₃₃BN₂

Guidance literature:: N,N-bis(2-bromophenyl)-N',N'-diphenylbenzene-1,4-diamine; With tert.-butyl lithium; In diethyl ether; pentane; at -78 - 0 ℃; Cooling with acetone-dry ice;

4,4,5,5-tetramethyl-2-(2-phenyl-naphthalen-1-yl)-[1,3,2]dioxaborolane; In diethyl ether; pentane; at -78 - 20 ℃; Reflux;

Reference yield:

: 67242-17-5
2,2’-dibromodiphenylamine

: 1347741-49-4
C₄₆H₃₃BN₂

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium carbonate / dimethyl sulfoxide / 48 h / 145 °C

2.1: tin(II) chloride monohydrate / ethanol; tetrahydrofuran / 5 h / Reflux

3.1: potassium carbonate; copper / 20 h / 200 °C

4.1: tert.-butyl lithium / diethyl ether; pentane / -78 - 0 °C / Cooling with acetone-dry ice

4.2: -78 - 20 °C / Reflux

With tin(II) chloride monohydrate; tert.-butyl lithium; copper; potassium carbonate; In tetrahydrofuran; diethyl ether; ethanol; dimethyl sulfoxide; pentane;

Reference yield:

: 350-46-9,178603-76-4
4-Fluoronitrobenzene

: 1347741-49-4
C₄₆H₃₃BN₂

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium carbonate / dimethyl sulfoxide / 48 h / 145 °C

2.1: tin(II) chloride monohydrate / ethanol; tetrahydrofuran / 5 h / Reflux

3.1: potassium carbonate; copper / 20 h / 200 °C

4.1: tert.-butyl lithium / diethyl ether; pentane / -78 - 0 °C / Cooling with acetone-dry ice

4.2: -78 - 20 °C / Reflux

With tin(II) chloride monohydrate; tert.-butyl lithium; copper; potassium carbonate; In tetrahydrofuran; diethyl ether; ethanol; dimethyl sulfoxide; pentane;