C₁₉H₃₀N₂O₅Si

Base Information

• Chemical Name: C₁₉H₃₀N₂O₅Si
• CAS No.: 1392005-77-4
• Molecular Formula: C₁₉H₃₀N₂O₅Si
• Molecular Weight: 394.543
• Mol file: 1392005-77-4.mol

Synonyms:C₁₉H₃₀N₂O₅Si

Chemical Property of C₁₉H₃₀N₂O₅Si

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₉H₃₀N₂O₅Si

There total 4 articles about C₁₉H₃₀N₂O₅Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

C24H38N2O7Si (1392005-76-3) → C19H30N2O5Si (1392005-77-4)

Guidance literature:

C₂₄H₃₈N₂O₇Si; With chloro-trimethyl-silane; phenol; In dichloromethane; at 20 ℃; for 0.333333h; Inert atmosphere;

With water; sodium hydroxide; In dichloromethane; Inert atmosphere;

DOI:10.1021/om300442e

Reference yield:

C9H19N3O2Si → C19H30N2O5Si (1392005-77-4)

Guidance literature:

Multi-step reaction with 6 steps

1.1: acetone / 16 h / Inert atmosphere; Reflux

2.1: hydrogenchloride / water / 6 h / Reflux

3.1: sodium hydroxide / water; methanol / 168 h / 20 °C / Inert atmosphere

4.1: thionyl chloride / -20 °C / Inert atmosphere; Reflux

5.1: 6-chloro-3-((dimethylamino)(dimethyliminio)methyl)-1H-benzo[d][1,2,3]triazol-3-ium-1-olatehexafluorophosphate(V); 4-methyl-morpholine / dichloromethane / 0.5 h / 20 °C / Inert atmosphere

6.1: chloro-trimethyl-silane; phenol / dichloromethane / 0.33 h / 20 °C / Inert atmosphere

6.2: Inert atmosphere

With 4-methyl-morpholine; hydrogenchloride; chloro-trimethyl-silane; thionyl chloride; 6-chloro-3-((dimethylamino)(dimethyliminio)methyl)-1H-benzo[d][1,2,3]triazol-3-ium-1-olatehexafluorophosphate(V); sodium hydroxide; phenol; In methanol; dichloromethane; water; acetone;

DOI:10.1021/om300442e

Reference yield:

C9H21NO2Si (1392043-65-0) → C19H30N2O5Si (1392005-77-4)

Guidance literature:

Multi-step reaction with 5 steps

1.1: hydrogenchloride / water / 6 h / Reflux

2.1: sodium hydroxide / water; methanol / 168 h / 20 °C / Inert atmosphere

3.1: thionyl chloride / -20 °C / Inert atmosphere; Reflux

4.1: 6-chloro-3-((dimethylamino)(dimethyliminio)methyl)-1H-benzo[d][1,2,3]triazol-3-ium-1-olatehexafluorophosphate(V); 4-methyl-morpholine / dichloromethane / 0.5 h / 20 °C / Inert atmosphere

5.1: chloro-trimethyl-silane; phenol / dichloromethane / 0.33 h / 20 °C / Inert atmosphere

5.2: Inert atmosphere

With 4-methyl-morpholine; hydrogenchloride; chloro-trimethyl-silane; thionyl chloride; 6-chloro-3-((dimethylamino)(dimethyliminio)methyl)-1H-benzo[d][1,2,3]triazol-3-ium-1-olatehexafluorophosphate(V); sodium hydroxide; phenol; In methanol; dichloromethane; water;

DOI:10.1021/om300442e

upstream raw materials:

diethyl methyl[(trimethylsilyl)methyl]malonate

C₉H₂₁NO₂Si

C₂₄H₃₈N₂O₇Si

Downstream raw materials:

C₂₄H₃₈N₂O₅Si

C₂₅H₄₀N₂O₅Si