(1R,3S)-1,2,2-trimethylcyclopentane-1,3-dicarboxylic aciddi(3-hydroxybenzoic acid) ester

Base Information

Chemical Name:(1R,3S)-1,2,2-trimethylcyclopentane-1,3-dicarboxylic aciddi(3-hydroxybenzoic acid) ester
CAS No.:183157-68-8
Molecular Formula:C₂₄H₂₄O₈
Molecular Weight:440.45
Hs Code.:

Synonyms:(1R,3S)-1,2,2-trimethylcyclopentane-1,3-dicarboxylic aciddi(3-hydroxybenzoic acid) ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1R,3S)-1,2,2-trimethylcyclopentane-1,3-dicarboxylic aciddi(3-hydroxybenzoic acid) ester

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Technology Process of (1R,3S)-1,2,2-trimethylcyclopentane-1,3-dicarboxylic aciddi(3-hydroxybenzoic acid) ester

There total 5 articles about (1R,3S)-1,2,2-trimethylcyclopentane-1,3-dicarboxylic aciddi(3-hydroxybenzoic acid) ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 183157-67-7
(1R,3S)-1,2,2-Trimethyl-cyclopentane-1,3-dicarboxylic acid bis-(3-tert-butoxycarbonyl-phenyl) ester

: 183157-68-8
(1R,3S)-1,2,2-trimethylcyclopentane-1,3-dicarboxylic aciddi(3-hydroxybenzoic acid) ester

Guidance literature:: With trifluoroacetic acid; In chloroform; Ambient temperature;
DOI:10.1016/0957-4166(96)00328-X

Reference yield:

: 124-83-4
D-(+)-camphoric acid

: 183157-68-8
(1R,3S)-1,2,2-trimethylcyclopentane-1,3-dicarboxylic aciddi(3-hydroxybenzoic acid) ester

Guidance literature:: Multi-step reaction with 3 steps

1: 66 percent / SOCl₂, DMF / CCl₄ / 3 h / Heating

2: 39 percent / Et₃N, DMAP / toluene / 35 h / Heating

3: 100 percent / TFA / CHCl₃ / Ambient temperature

With dmap; thionyl chloride; triethylamine; N,N-dimethyl-formamide; trifluoroacetic acid; In tetrachloromethane; chloroform; toluene;
DOI:10.1016/0957-4166(96)00328-X

Reference yield:

: 99-06-9
3-Carboxyphenol

: 183157-68-8
(1R,3S)-1,2,2-trimethylcyclopentane-1,3-dicarboxylic aciddi(3-hydroxybenzoic acid) ester

Guidance literature:: Multi-step reaction with 3 steps

1: 56 percent / benzene / 0.5 h / Heating

2: 39 percent / Et₃N, DMAP / toluene / 35 h / Heating

3: 100 percent / TFA / CHCl₃ / Ambient temperature

With dmap; triethylamine; trifluoroacetic acid; In chloroform; toluene; benzene;
DOI:10.1016/0957-4166(96)00328-X