N-(7-{[3-O-(aminocarbonyl)-6-deoxy-5-C-methyl-4-O-methyl-α-L-lyxohexopyranosyl]oxy}-4-hydroxy-8-methyl-2-oxo-2H-1-benzopyran-3-yl)cyclohexanecarboxamide

Base Information

Chemical Name:N-(7-{[3-O-(aminocarbonyl)-6-deoxy-5-C-methyl-4-O-methyl-α-L-lyxohexopyranosyl]oxy}-4-hydroxy-8-methyl-2-oxo-2H-1-benzopyran-3-yl)cyclohexanecarboxamide
CAS No.:1449759-54-9
Molecular Formula:C₂₆H₃₄N₂O₁₀
Molecular Weight:534.563
Hs Code.:

N-(7-{[3-O-(aminocarbonyl)-6-deoxy-5-C-methyl-4-O-methyl-α-L-lyxohexopyranosyl]oxy}-4-hydroxy-8-methyl-2-oxo-2H-1-benzopyran-3-yl)cyclohexanecarboxamide

Synonyms:N-(7-{[3-O-(aminocarbonyl)-6-deoxy-5-C-methyl-4-O-methyl-α-L-lyxohexopyranosyl]oxy}-4-hydroxy-8-methyl-2-oxo-2H-1-benzopyran-3-yl)cyclohexanecarboxamide

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Chemical Property of N-(7-{[3-O-(aminocarbonyl)-6-deoxy-5-C-methyl-4-O-methyl-α-L-lyxohexopyranosyl]oxy}-4-hydroxy-8-methyl-2-oxo-2H-1-benzopyran-3-yl)cyclohexanecarboxamide

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Technology Process of N-(7-{[3-O-(aminocarbonyl)-6-deoxy-5-C-methyl-4-O-methyl-α-L-lyxohexopyranosyl]oxy}-4-hydroxy-8-methyl-2-oxo-2H-1-benzopyran-3-yl)cyclohexanecarboxamide

There total 5 articles about N-(7-{[3-O-(aminocarbonyl)-6-deoxy-5-C-methyl-4-O-methyl-α-L-lyxohexopyranosyl]oxy}-4-hydroxy-8-methyl-2-oxo-2H-1-benzopyran-3-yl)cyclohexanecarboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1489273-46-2
C₂₈H₃₆N₂O₁₁

: 1449759-54-9
N-(7-{[3-O-(aminocarbonyl)-6-deoxy-5-C-methyl-4-O-methyl-α-L-lyxohexopyranosyl]oxy}-4-hydroxy-8-methyl-2-oxo-2H-1-benzopyran-3-yl)cyclohexanecarboxamide

Guidance literature:: With sodium cyanide; In methanol; at 25 ℃;
DOI:10.1016/j.bmc.2013.06.042

Reference yield:

: 116635-17-7
1-<(2,6-dimethyl-4-oxo-4H-<1>benzopyrano<3,4-d>oxazol-7-yl)oxy>-2-acetoxy-4-methoxy-5,5-dimethyl-3-tetrahydropyranyl 5-methyl-1H-pyrrole-2-carboxylate

: 1449759-54-9
N-(7-{[3-O-(aminocarbonyl)-6-deoxy-5-C-methyl-4-O-methyl-α-L-lyxohexopyranosyl]oxy}-4-hydroxy-8-methyl-2-oxo-2H-1-benzopyran-3-yl)cyclohexanecarboxamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: ethanol / 3 h / Reflux

2.1: dicyclohexyl-carbodiimide; 4-pyrrolidin-1-ylpyridine / ethanol / 0.5 h / 25 °C

2.2: 25 °C

3.1: sodium cyanide / methanol / 25 °C

With sodium cyanide; 4-pyrrolidin-1-ylpyridine; dicyclohexyl-carbodiimide; In methanol; ethanol;
DOI:10.1016/j.bmc.2013.06.042

Reference yield:

: 1476-53-5,6990-02-9,18656-99-0
sodium novobiocin

: 1449759-54-9
N-(7-{[3-O-(aminocarbonyl)-6-deoxy-5-C-methyl-4-O-methyl-α-L-lyxohexopyranosyl]oxy}-4-hydroxy-8-methyl-2-oxo-2H-1-benzopyran-3-yl)cyclohexanecarboxamide

Guidance literature:: Multi-step reaction with 5 steps

1.1: hydrogenchloride / water

2.1: pyridine / 24 h / Reflux

3.1: ethanol / 3 h / Reflux

4.1: dicyclohexyl-carbodiimide; 4-pyrrolidin-1-ylpyridine / ethanol / 0.5 h / 25 °C

4.2: 25 °C

5.1: sodium cyanide / methanol / 25 °C

With pyridine; hydrogenchloride; sodium cyanide; 4-pyrrolidin-1-ylpyridine; dicyclohexyl-carbodiimide; In methanol; ethanol; water;
DOI:10.1016/j.bmc.2013.06.042