C₄₇H₄₆O₈

Base Information

Chemical Name:C₄₇H₄₆O₈
CAS No.:1393673-72-7
Molecular Formula:C₄₇H₄₆O₈
Molecular Weight:738.877
Hs Code.:

C<sub>47</sub>H<sub>46</sub>O<sub>8</sub>

Synonyms:C₄₇H₄₆O₈

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Chemical Property of C₄₇H₄₆O₈

Chemical Property:

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Technology Process of C₄₇H₄₆O₈

There total 4 articles about C₄₇H₄₆O₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 1393673-71-6
C₄₇H₄₇FO₈

: 1393673-72-7
C₄₇H₄₆O₈

Guidance literature:: With potassium hydride; In N,N-dimethyl-formamide; at 20 ℃; for 2h; Inert atmosphere;
DOI:10.1039/c2cc33704e

Reference yield:

: C₂₃H₂₂O₄

: 1393673-72-7
C₄₇H₄₆O₈

Guidance literature:: Multi-step reaction with 5 steps

1.1: 1H-imidazole / N,N-dimethyl-formamide / 2 h / 0 °C / Inert atmosphere

2.1: n-butyllithium / hexane; tetrahydrofuran / 1 h / -78 °C / Inert atmosphere

2.2: 0.25 h / -78 °C / Inert atmosphere

3.1: N-ethyl-N,N-diisopropylamine; tetra-(n-butyl)ammonium iodide / 15 h / 20 °C

4.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 14 h / 20 °C / Inert atmosphere

5.1: potassium hydride / N,N-dimethyl-formamide / 2 h / 20 °C / Inert atmosphere

With 1H-imidazole; n-butyllithium; tetrabutyl ammonium fluoride; tetra-(n-butyl)ammonium iodide; potassium hydride; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; hexane; N,N-dimethyl-formamide;
DOI:10.1039/c2cc33704e

Reference yield:

: 372-38-3
1,3,5-trifluorobenzene

: 1393673-72-7
C₄₇H₄₆O₈

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium hydride / hexane; mineral oil; 1-methyl-pyrrolidin-2-one / 1 h / 0 °C / Inert atmosphere

1.2: 4 h / 20 - 100 °C / Inert atmosphere

2.1: n-butyllithium / hexane; tetrahydrofuran / 1 h / -78 °C / Inert atmosphere

2.2: 0.25 h / -78 °C / Inert atmosphere

3.1: N-ethyl-N,N-diisopropylamine; tetra-(n-butyl)ammonium iodide / 15 h / 20 °C

4.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 14 h / 20 °C / Inert atmosphere

5.1: potassium hydride / N,N-dimethyl-formamide / 2 h / 20 °C / Inert atmosphere

With n-butyllithium; tetrabutyl ammonium fluoride; tetra-(n-butyl)ammonium iodide; potassium hydride; sodium hydride; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; 1-methyl-pyrrolidin-2-one; hexane; N,N-dimethyl-formamide; mineral oil;
DOI:10.1039/c2cc33704e