2-(10-(4-(biphenylcarbonyl)-1,4-diazepan-1-yl)decyl)-3-methylnaphthalene-1,4-dione

Base Information

Chemical Name:2-(10-(4-(biphenylcarbonyl)-1,4-diazepan-1-yl)decyl)-3-methylnaphthalene-1,4-dione
CAS No.:1594439-43-6
Molecular Formula:C₃₉H₄₆N₂O₃
Molecular Weight:590.806
Hs Code.:

Synonyms:2-(10-(4-(biphenylcarbonyl)-1,4-diazepan-1-yl)decyl)-3-methylnaphthalene-1,4-dione

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Chemical Property of 2-(10-(4-(biphenylcarbonyl)-1,4-diazepan-1-yl)decyl)-3-methylnaphthalene-1,4-dione

Chemical Property:

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Technology Process of 2-(10-(4-(biphenylcarbonyl)-1,4-diazepan-1-yl)decyl)-3-methylnaphthalene-1,4-dione

There total 6 articles about 2-(10-(4-(biphenylcarbonyl)-1,4-diazepan-1-yl)decyl)-3-methylnaphthalene-1,4-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 815650-69-2
C₁₈H₂₀N₂O

: 1374028-67-7
2-(10-bromodecyl)-3-methylnaphthalene-1,4-dione

: 1594439-43-6
2-(10-(4-(biphenylcarbonyl)-1,4-diazepan-1-yl)decyl)-3-methylnaphthalene-1,4-dione

Guidance literature:: With tetra-(n-butyl)ammonium iodide; In acetonitrile; for 24h; Reflux;
DOI:10.1016/j.bmcl.2014.02.072

Reference yield:

: 58-27-5,34524-96-4
menadione

: 1594439-43-6
2-(10-(4-(biphenylcarbonyl)-1,4-diazepan-1-yl)decyl)-3-methylnaphthalene-1,4-dione

Guidance literature:: Multi-step reaction with 2 steps

1.1: ammonium peroxydisulfate / water / 1 h

1.2: 4 h / 75 °C / Darkness

2.1: tetra-(n-butyl)ammonium iodide / acetonitrile / 24 h / Reflux

With ammonium peroxydisulfate; tetra-(n-butyl)ammonium iodide; In water; acetonitrile;
DOI:10.1016/j.bmcl.2014.02.072

Reference yield:

: 117009-97-9
benzyl 1,4-diazepane-1-carboxylate

: 1594439-43-6
2-(10-(4-(biphenylcarbonyl)-1,4-diazepan-1-yl)decyl)-3-methylnaphthalene-1,4-dione

Guidance literature:: Multi-step reaction with 3 steps

1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 5 h / 0 - 20 °C

2: palladium 10% on activated carbon; hydrogen / methanol / 20 °C

3: tetra-(n-butyl)ammonium iodide / acetonitrile / 24 h / Reflux

With palladium 10% on activated carbon; hydrogen; tetra-(n-butyl)ammonium iodide; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In methanol; dichloromethane; acetonitrile;
DOI:10.1016/j.bmcl.2014.02.072