N-(2,6-dimethyl-4-heptafluoroisopropyl)phenyl-3-(phenylthiocarbonylamino)benzamide

Base Information

Chemical Name:N-(2,6-dimethyl-4-heptafluoroisopropyl)phenyl-3-(phenylthiocarbonylamino)benzamide
CAS No.:862134-89-2
Molecular Formula:C₂₅H₁₉F₇N₂OS
Molecular Weight:528.493
Hs Code.:

Synonyms:N-(2,6-dimethyl-4-heptafluoroisopropyl)phenyl-3-(phenylthiocarbonylamino)benzamide

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Chemical Property of N-(2,6-dimethyl-4-heptafluoroisopropyl)phenyl-3-(phenylthiocarbonylamino)benzamide

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Technology Process of N-(2,6-dimethyl-4-heptafluoroisopropyl)phenyl-3-(phenylthiocarbonylamino)benzamide

There total 13 articles about N-(2,6-dimethyl-4-heptafluoroisopropyl)phenyl-3-(phenylthiocarbonylamino)benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

: 862130-26-5
N-(2,6-dimethyl-4-heptafluoroisopropyl)phenyl-3-(benzoylamino)benzamide

: 862134-90-5
N-(2,6-dimethyl-4-heptafluoroisopropyl)phenyl-3-(phenylthiocarbonylamino)benzthioamide

: 862134-89-2
N-(2,6-dimethyl-4-heptafluoroisopropyl)phenyl-3-(phenylthiocarbonylamino)benzamide

Guidance literature:: With Lawessons reagent; In toluene; at 70 ℃; for 6h;

Reference yield:

: 914463-26-6
N-[2,6-dimethyl-4-{1-hydroxy-2,2,2-trifluoro-1-(trifluoromethyl)-ethyl}phenyl] 3-nitrobenzamide

: 862134-90-5
N-(2,6-dimethyl-4-heptafluoroisopropyl)phenyl-3-(phenylthiocarbonylamino)benzthioamide

: 862134-89-2
N-(2,6-dimethyl-4-heptafluoroisopropyl)phenyl-3-(phenylthiocarbonylamino)benzamide

Guidance literature:: Multi-step reaction with 4 steps

1: hydrogen / palladium 10% on activated carbon / methanol / 20 °C

2: pyridine / tetrahydrofuran / 20 °C

3: 2,2-difluoro-1,3-dimethyl-imidazolidine / dichloromethane / 8 h / 20 °C

4: Lawessons reagent / toluene / 6 h / 70 °C

With Lawessons reagent; pyridine; hydrogen; 2,2-difluoro-1,3-dimethyl-imidazolidine; palladium 10% on activated carbon; In tetrahydrofuran; methanol; dichloromethane; toluene;

Reference yield:

: N-[2,6-dimethyl-4-{1-hydroxy-2,2,2-trifluoro-1-(trifluoromethyl)-ethyl}phenyl] 3-(benzoylamino)benzamide

: 862134-90-5
N-(2,6-dimethyl-4-heptafluoroisopropyl)phenyl-3-(phenylthiocarbonylamino)benzthioamide

: 862134-89-2
N-(2,6-dimethyl-4-heptafluoroisopropyl)phenyl-3-(phenylthiocarbonylamino)benzamide

Guidance literature:: Multi-step reaction with 2 steps

1: 2,2-difluoro-1,3-dimethyl-imidazolidine / dichloromethane / 8 h / 20 °C

2: Lawessons reagent / toluene / 6 h / 70 °C

With Lawessons reagent; 2,2-difluoro-1,3-dimethyl-imidazolidine; In dichloromethane; toluene;