[Zn(Et)(κ2-η1(π)-2,2-bis(3,5-dimethylpyrazol-1-yl)-1,1-diphenylethylcyclopentadienyl)]

Base Information

Chemical Name:[Zn(Et)(κ2-η1(π)-2,2-bis(3,5-dimethylpyrazol-1-yl)-1,1-diphenylethylcyclopentadienyl)]
CAS No.:1215085-52-1
Molecular Formula:C₃₁H₃₄N₄Zn
Molecular Weight:528.028
Hs Code.:

Synonyms:[Zn(Et)(κ2-η1(π)-2,2-bis(3,5-dimethylpyrazol-1-yl)-1,1-diphenylethylcyclopentadienyl)]

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Chemical Property of [Zn(Et)(κ2-η1(π)-2,2-bis(3,5-dimethylpyrazol-1-yl)-1,1-diphenylethylcyclopentadienyl)]

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Technology Process of [Zn(Et)(κ2-η1(π)-2,2-bis(3,5-dimethylpyrazol-1-yl)-1,1-diphenylethylcyclopentadienyl)]

There total 2 articles about [Zn(Et)(κ2-η1(π)-2,2-bis(3,5-dimethylpyrazol-1-yl)-1,1-diphenylethylcyclopentadienyl)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 557-20-0
diethylzinc

: 1215085-52-1
[Zn(Et)(κ2-η1(π)-2,2-bis(3,5-dimethylpyrazol-1-yl)-1,1-diphenylethylcyclopentadienyl)]

Guidance literature:: With C₅H₅C(C₆H₅)2CH(C₃HN₂(CH₃)2)2; In toluene; (N2); a soln. of ligand cooled to -70°C, a soln. of Zn compd. added, allowed to warm to room temp. and stirred; evapd. (vac.), washed (hexane), recrystd. (toluene, -26°C); elem.anal.;
DOI:10.1021/ic902399r

Reference yield:

: 1215085-46-3
[Mg(Et)(κ2-η5-bpzcp)]

: 7646-85-7,24359-56-6
zinc(II) chloride

: 1215085-52-1
[Zn(Et)(κ2-η1(π)-2,2-bis(3,5-dimethylpyrazol-1-yl)-1,1-diphenylethylcyclopentadienyl)]

Guidance literature:: In diethyl ether; toluene; (N2); a soln. of Mg compd. in dry toluene reacted with an ether soln. ofZnCl2, stirred; evapd. (vac.), extd. and recrystd. from toluene;
DOI:10.1021/ic902399r