N-benzoyl-N'-(1,2-dimorpholino)ethylidenemethoxyformamidine

Base Information

• Chemical Name: N-benzoyl-N'-(1,2-dimorpholino)ethylidenemethoxyformamidine
• CAS No.: 74362-22-4
• Molecular Formula: C₁₉H₂₆N₄O₄
• Molecular Weight: 374.44
• Mol file: 74362-22-4.mol

Synonyms:N-benzoyl-N'-(1,2-dimorpholino)ethylidenemethoxyformamidine

Chemical Property of N-benzoyl-N'-(1,2-dimorpholino)ethylidenemethoxyformamidine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N-benzoyl-N'-(1,2-dimorpholino)ethylidenemethoxyformamidine

There total 5 articles about N-benzoyl-N'-(1,2-dimorpholino)ethylidenemethoxyformamidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

1-benzoyl-4,5-dimorpholino-2-methoxy-4,5-dihydroimidazole (74362-14-4) → N-benzoyl-N'-(1,2-dimorpholino)ethylidenemethoxyformamidine (74362-22-4)

Guidance literature:

With triethylamine hydrochloride; In toluene; for 3h; Heating;

DOI:10.1002/jhet.5570170120

Reference yield:

N-(iminomethoxymethyl)benzamide (58476-79-2) → N-benzoyl-N'-(1,2-dimorpholino)ethylidenemethoxyformamidine (74362-22-4)

Guidance literature:

Multi-step reaction with 2 steps

1: 30 percent / triethylamine / CH₂Cl₂

2: 93 percent / triethylamine hydrochloride / toluene / 3 h / Heating

With triethylamine hydrochloride; triethylamine; In dichloromethane; toluene;

DOI:10.1002/jhet.5570170120

Reference yield:

1,2-dimorpholinoethylene (26727-98-0) → N-benzoyl-N'-(1,2-dimorpholino)ethylidenemethoxyformamidine (74362-22-4)

Guidance literature:

Multi-step reaction with 2 steps

1: 87 percent / pyridine / CH₂Cl₂ / 0.75 h / Ambient temperature

2: 93 percent / triethylamine hydrochloride / toluene / 3 h / Heating

With pyridine; triethylamine hydrochloride; In dichloromethane; toluene;

DOI:10.1002/jhet.5570170120

upstream raw materials:

1-benzoyl-4,5-dimorpholino-2-methoxy-4,5-dihydroimidazole

1,2-dimorpholinoethylene

N-(iminomethoxymethyl)benzamide

N-benzoyl-N'-chloromethoxyformamidine