[1,1'-Biphenyl]-2,2'-diol, 2-(4-methylbenzenesulfonate)

Base Information

Chemical Name:[1,1'-Biphenyl]-2,2'-diol, 2-(4-methylbenzenesulfonate)
CAS No.:938058-83-4
Molecular Formula:C₁₉H₁₆O₄S
Molecular Weight:340.4
Hs Code.:
DSSTox Substance ID:DTXSID701206466
Nikkaji Number:J2.451.521D

Synonyms:DTXSID701206466;938058-83-4

Suppliers and Price of [1,1'-Biphenyl]-2,2'-diol, 2-(4-methylbenzenesulfonate)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of [1,1'-Biphenyl]-2,2'-diol, 2-(4-methylbenzenesulfonate)

Chemical Property:

XLogP3:4.7
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:4
Exact Mass:340.07693016
Heavy Atom Count:24
Complexity:490

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC1=CC=C(C=C1)S(=O)(=O)OC2=CC=CC=C2C3=CC=CC=C3O

Technology Process of [1,1'-Biphenyl]-2,2'-diol, 2-(4-methylbenzenesulfonate)

There total 1 articles about [1,1'-Biphenyl]-2,2'-diol, 2-(4-methylbenzenesulfonate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1806-29-7
2,2'-dihydroxybiphenyl

: 98-59-9
p-toluenesulfonyl chloride

: 938058-83-4
2'-hydroxy-[1,1'-biphenyl]-2-yl 4-methylbenzenesulfonate

Guidance literature:: With dmap; triethylamine; In dichloromethane; at 20 ℃; for 8h;
DOI:10.1002/ejoc.200600962

Reference yield: 70.0%

: 938058-83-4
2'-hydroxy-[1,1'-biphenyl]-2-yl 4-methylbenzenesulfonate

: 80-48-8
methyl p-toluene sulfonate

: 77897-02-0
2-hydroxy-2'-methyl-1,1'-biphenyl

Guidance literature:: With 1,1'-bis-(diphenylphosphino)ferrocene; (1,2-dimethoxyethane)dichloronickel(II); tetra-(n-butyl)ammonium iodide; lithium chloride; zinc; In N,N-dimethyl acetamide; at 40 ℃; for 12h; Schlenk technique; Inert atmosphere; Sealed tube;
DOI:10.1039/c7cc06106d

Reference yield:

: 556-64-9
methyl thiocyanate

: 938058-83-4
2'-hydroxy-[1,1'-biphenyl]-2-yl 4-methylbenzenesulfonate

: C₂₀H₁₅NO₄S

Guidance literature:: With aluminum (III) chloride; boron trichloride; In dichloromethane; 1,2-dichloro-ethane; at 80 ℃; for 24h; Inert atmosphere;
DOI:10.1021/acs.joc.0c00458