trans-[Fe(CO)3(PMe₃)2(Me)]BPh₄

Base Information

Chemical Name:trans-[Fe(CO)3(PMe₃)2(Me)]BPh₄
CAS No.:82660-90-0
Molecular Formula:C₁₀H₂₁FeO₃P₂*C₂₄H₂₀B
Molecular Weight:626.303
Hs Code.:

trans-[Fe(CO)3(PMe<sub>3</sub>)2(Me)]BPh<sub>4</sub>

Synonyms:trans-[Fe(CO)3(PMe₃)2(Me)]BPh₄

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Chemical Property of trans-[Fe(CO)3(PMe₃)2(Me)]BPh₄

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Technology Process of trans-[Fe(CO)3(PMe₃)2(Me)]BPh₄

There total 2 articles about trans-[Fe(CO)3(PMe₃)2(Me)]BPh₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 33542-07-3
cis,trans-[dicarbonylbis(trimethylphosphine)(methyl)iodoiron(II)]

: 143-66-8
sodium tetraphenyl borate

: 82660-90-0
trans-[Fe(CO)3(PMe₃)2(Me)]BPh₄

Guidance literature:: With carbon monoxide; In methanol; soln. of FeICH3(CO)2(PMe3)2 in methanol was mixed with NaBPh4 in methanol, CO was bubbled into this mixt. at room temp.; solid was filtered off, washed with methanol, dried under vac.; elem. anal.;

Reference yield:

: 78306-61-3
cis,trans-FeI(CO)2(PMe₃)2(COMe)

: 143-66-8
sodium tetraphenyl borate

: 82660-90-0
trans-[Fe(CO)3(PMe₃)2(Me)]BPh₄

Guidance literature:: In dichloromethane; pptn.;

Reference yield: 100.0%

: 82660-90-0
trans-[Fe(CO)3(PMe₃)2(Me)]BPh₄

: 94235-66-2,57322-08-4
Methylphenylphosphinsaeuremethylester

: 94249-32-8
Fe(COCH₃)(CO)2(C₆H₅P(CH₃)(OCH₃))(P(CH₃)3)2⁽¹⁺⁾*B(C₆H₅)4^(1-)=(Fe(COCH₃)(CO)2(C₆H₅P(CH₃)(OCH₃))(P(CH₃)3)2)(B(C₆H₅)4)

Guidance literature:: In dichloromethane; soln. of FeCH3(CO)3(PMe3)2(BPh4) in CH2Cl2 was cooled to -20°C and reacted with PhP(Me)(OMe) in CH2Cl2 for 1 h; cold ether was added, ppt. was collected, washed with cold ether;