((3aR,5R,6S,6aR)-2,2-Dimethyl-6-(((Trifluoromethyl)Sulfonyl)Oxy)Tetrahydrofuro[2,3-D][1,3]Dioxol-5-Yl)Methyl 4-Methylbenzoate

Base Information

Chemical Name:((3aR,5R,6S,6aR)-2,2-Dimethyl-6-(((Trifluoromethyl)Sulfonyl)Oxy)Tetrahydrofuro[2,3-D][1,3]Dioxol-5-Yl)Methyl 4-Methylbenzoate
CAS No.:75096-61-6
Molecular Formula:C₁₇H₁₉F₃O₈S
Molecular Weight:440.394
Hs Code.:
Mol file:75096-61-6.mol

Synonyms:1,2-O-isopropylidene-5-O-(4-methylbenzoyl)-3-O-trifluoromethanesulfonyl-α-D-xylofuranose

Suppliers and Price of ((3aR,5R,6S,6aR)-2,2-Dimethyl-6-(((Trifluoromethyl)Sulfonyl)Oxy)Tetrahydrofuro[2,3-D][1,3]Dioxol-5-Yl)Methyl 4-Methylbenzoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
((3aR,5R,6S,6aR)-2,2-Dimethyl-6-(((trifluoromethyl)sulfonyl)oxy)tetrahydrofuro[2,3-d][1,3]dioxol-5-yl)methyl4-methylbenzoate 95+%
5g
$ 1786.00

Crysdot
((3aR,5R,6S,6aR)-2,2-Dimethyl-6-(((trifluoromethyl)sulfonyl)oxy)tetrahydrofuro[2,3-d][1,3]dioxol-5-yl)methyl4-methylbenzoate 95+%
1g
$ 594.00

Total 4 raw suppliers

Chemical Property of ((3aR,5R,6S,6aR)-2,2-Dimethyl-6-(((Trifluoromethyl)Sulfonyl)Oxy)Tetrahydrofuro[2,3-D][1,3]Dioxol-5-Yl)Methyl 4-Methylbenzoate

Chemical Property:

Purity/Quality:

97% ^*data from raw suppliers

((3aR,5R,6S,6aR)-2,2-Dimethyl-6-(((trifluoromethyl)sulfonyl)oxy)tetrahydrofuro[2,3-d][1,3]dioxol-5-yl)methyl4-methylbenzoate 95+% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of ((3aR,5R,6S,6aR)-2,2-Dimethyl-6-(((Trifluoromethyl)Sulfonyl)Oxy)Tetrahydrofuro[2,3-D][1,3]Dioxol-5-Yl)Methyl 4-Methylbenzoate

There total 4 articles about ((3aR,5R,6S,6aR)-2,2-Dimethyl-6-(((Trifluoromethyl)Sulfonyl)Oxy)Tetrahydrofuro[2,3-D][1,3]Dioxol-5-Yl)Methyl 4-Methylbenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 358-23-6
trifluoromethylsulfonic anhydride

: 75096-60-5
1,2-O-isopropylidene-5-O-(4-toluoyl)-D-xylofuranose

: 75096-61-6
1,2-O-isopropylidene-5-O-(4-methylbenzoyl)-3-O-trifluoromethanesulfonyl-α-D-xylofuranose

Guidance literature:: With pyridine; In 1,2-dichloro-ethane; at -10 ℃; for 0.5h;
DOI:10.1055/s-1980-29120

Reference yield:

: 20031-21-4
1,2-O-isopropylidene-α-D-xylose

: 75096-61-6
1,2-O-isopropylidene-5-O-(4-methylbenzoyl)-3-O-trifluoromethanesulfonyl-α-D-xylofuranose

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine

2: DMAP / CH₂Cl₂ / Ambient temperature

With pyridine; dmap; In dichloromethane;
DOI:10.1080/07328319708006225

Reference yield:

: 874-60-2
4-methyl-benzoyl chloride

: 75096-61-6
1,2-O-isopropylidene-5-O-(4-methylbenzoyl)-3-O-trifluoromethanesulfonyl-α-D-xylofuranose

Guidance literature:: Multi-step reaction with 2 steps

1: 97 percent / pyridine / 1 h / 0 °C

2: 93 percent / pyridine / 1,2-dichloro-ethane / 0.5 h / -10 °C

With pyridine; In 1,2-dichloro-ethane;
DOI:10.1055/s-1980-29120