1-{2-O-[(3-acetoxypropoxy)methyl]-β-D-ribofuranosyl}-N⁴-benzoylcytosine

Base Information

Chemical Name:1-{2-O-[(3-acetoxypropoxy)methyl]-β-D-ribofuranosyl}-N⁴-benzoylcytosine
CAS No.:933063-87-7
Molecular Formula:C₂₂H₂₇N₃O₉
Molecular Weight:477.471
Hs Code.:

1-{2-O-[(3-acetoxypropoxy)methyl]-β-D-ribofuranosyl}-N<sup>4</sup>-benzoylcytosine

Synonyms:1-{2-O-[(3-acetoxypropoxy)methyl]-β-D-ribofuranosyl}-N⁴-benzoylcytosine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-{2-O-[(3-acetoxypropoxy)methyl]-β-D-ribofuranosyl}-N⁴-benzoylcytosine

Chemical Property:

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Technology Process of 1-{2-O-[(3-acetoxypropoxy)methyl]-β-D-ribofuranosyl}-N⁴-benzoylcytosine

There total 2 articles about 1-{2-O-[(3-acetoxypropoxy)methyl]-β-D-ribofuranosyl}-N⁴-benzoylcytosine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 933063-83-3
1-{2-O-[(3-acetoxypropoxy)methyl]-3,5-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)-β-D-ribofuranosyl}-N⁴-benzoylcytosine

: 933063-87-7
1-{2-O-[(3-acetoxypropoxy)methyl]-β-D-ribofuranosyl}-N⁴-benzoylcytosine

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 20 ℃;
DOI:10.1135/cccc20060804

Reference yield:

: 93185-18-3
3-(hydroxymethoxy)propan-1-ol diacetate

: 933063-87-7
1-{2-O-[(3-acetoxypropoxy)methyl]-β-D-ribofuranosyl}-N⁴-benzoylcytosine

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / tin tetrachloride / 1,2-dichloro-ethane / 0.33 h / -12 °C

2: 89 percent / Bu₄NF*3H₂O / tetrahydrofuran / 20 °C

With tetrabutyl ammonium fluoride; tin(IV) chloride; In tetrahydrofuran; 1,2-dichloro-ethane;
DOI:10.1135/cccc20060804