3-(12-tert-butoxycarbonylamino-dodecyloxy)-5-(2-tert-butoxycarbonylamino-ethoxy)-benzoic acid methyl ester

Base Information

• Chemical Name: 3-(12-tert-butoxycarbonylamino-dodecyloxy)-5-(2-tert-butoxycarbonylamino-ethoxy)-benzoic acid methyl ester
• CAS No.: 849100-70-5
• Molecular Formula: C₃₂H₅₄N₂O₈
• Molecular Weight: 594.789

Synonyms:3-(12-tert-butoxycarbonylamino-dodecyloxy)-5-(2-tert-butoxycarbonylamino-ethoxy)-benzoic acid methyl ester

Chemical Property of 3-(12-tert-butoxycarbonylamino-dodecyloxy)-5-(2-tert-butoxycarbonylamino-ethoxy)-benzoic acid methyl ester

Chemical Property:

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Technology Process of 3-(12-tert-butoxycarbonylamino-dodecyloxy)-5-(2-tert-butoxycarbonylamino-ethoxy)-benzoic acid methyl ester

There total 3 articles about 3-(12-tert-butoxycarbonylamino-dodecyloxy)-5-(2-tert-butoxycarbonylamino-ethoxy)-benzoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

12-((tert-butoxycarbonyl)amino)dodecyl methanesulfonate (154371-97-8) + 3-hydroxy-5-[2-(Boc-amino)ethoxy]benzoic acid methylester (849100-67-0) → 3-(12-tert-butoxycarbonylamino-dodecyloxy)-5-(2-tert-butoxycarbonylamino-ethoxy)-benzoic acid methyl ester (849100-70-5)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 40 ℃; for 144h;

DOI:10.1002/ejoc.200400609

Reference yield:

1-carbomethoxy-3,5-dihydroxybenzene (2150-44-9) → 3-(12-tert-butoxycarbonylamino-dodecyloxy)-5-(2-tert-butoxycarbonylamino-ethoxy)-benzoic acid methyl ester (849100-70-5)

Guidance literature:

Multi-step reaction with 2 steps

1: 26 percent / K₂CO₃ / dimethylformamide / 48 h / 40 °C

2: 85 percent / potassium carbonate / dimethylformamide / 144 h / 40 °C

With potassium carbonate; In N,N-dimethyl-formamide;

DOI:10.1002/ejoc.200400609

Reference yield:

2-(tert-butoxycarbonylamino)ethyl bromide (39684-80-5) → 3-(12-tert-butoxycarbonylamino-dodecyloxy)-5-(2-tert-butoxycarbonylamino-ethoxy)-benzoic acid methyl ester (849100-70-5)

Guidance literature:

Multi-step reaction with 2 steps

1: 26 percent / K₂CO₃ / dimethylformamide / 48 h / 40 °C

2: 85 percent / potassium carbonate / dimethylformamide / 144 h / 40 °C

With potassium carbonate; In N,N-dimethyl-formamide;

DOI:10.1002/ejoc.200400609

upstream raw materials:

12-((tert-butoxycarbonyl)amino)dodecyl methanesulfonate

3-hydroxy-5-[2-(Boc-amino)ethoxy]benzoic acid methylester

1-carbomethoxy-3,5-dihydroxybenzene

2-(tert-butoxycarbonylamino)ethyl bromide

Downstream raw materials:

3-(2-tert-butoxycarbonylamino-ethoxy)-5-(2-{3-[12-(4-nitro-phenylamino)-dodecyloxy]-5-[2-(4-nitro-phenylamino)-ethoxy]-benzoylamino}-ethoxy)-benzoic acid methyl ester

3-[12-(4-nitro-phenylamino)-dodecyloxy]-5-[2-(4-nitro-phenylamino)-ethoxy]-benzoic acid

3-[12-(4-nitro-phenylamino)-dodecyloxy]-5-[2-(4-nitro-phenylamino)-ethoxy]-benzoic acid methyl ester

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